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Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin. PubMed SCIE
期刊论文 | 2019 , 45 (2) , 273-281 | Drug development and industrial pharmacy
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Abstract :

The aim of this work is to develop curcumin-loaded hollow mesoporous silica microspheres (HMSMs@curcumin) to improve the poor oral bioavailability of curcumin. Hollow mesoporous silica microspheres (HMSMs) were synthesized in facile route using a hard template. HMSMs and HMSMs@curcumin were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), nitrogen adsorption/desorption measurements, differential scanning calorimetry (DSC), Fourier transform infrared (FTIR) and X-ray diffraction (XRD). In addition, to demonstrate the potential application of the HMSMs@curcumin, cytotoxicity, in vitro release behavior and in vivo pharmacokinetics of curcumin loaded in these HMSMs were investigated by using of Caco-2 cells and Sprague-Dawley (SD) rats, respectively. These mono-dispersed HMSMs exhibited high drug loading ratio and encapsulation efficiency due to the mesoporous shell and hollow core. The excellent characteristics of HMSMs such as mono-dispersed morphology, smooth surface, uniform, ordered and size-narrowing mesopores resulted in a good in vitro release profile of curcumin from HMSMs@curcumin. Moreover, an impressive improvement in the oral absorption of curcumin and prolonged systemic circulation time were achieved in the in vivo animal studies. In addition, the good biocompatibility of developed HMSMs with Caco-2 cells was confirmed based on the in vitro cytotoxicity assay. In conclusion, this system demonstrated a great potential for efficiently delivery of curcumin in vitro and in vivo, suggesting a good prospect for its application in clinic for therapeutic drug delivery in future.

Keyword :

Cytotoxicity Hollow mesoporous silica microspheres (HMSMs) Curcumin In vivo drug delivery In vitro drug release

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GB/T 7714 Gao Yang , Ding Shujiang , Huang Xiaoyan et al. Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin. [J]. | Drug development and industrial pharmacy , 2019 , 45 (2) : 273-281 .
MLA Gao Yang et al. "Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin." . | Drug development and industrial pharmacy 45 . 2 (2019) : 273-281 .
APA Gao Yang , Ding Shujiang , Huang Xiaoyan , Fan Zhaoyang , Sun Jianmei , Hai Yang et al. Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin. . | Drug development and industrial pharmacy , 2019 , 45 (2) , 273-281 .
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Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption SCIE
期刊论文 | 2019 , 7 (7) , 3039-3045 | JOURNAL OF MATERIALS CHEMISTRY A
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While non-noble transition metal nanoparticles are widely explored in the field of solar energy harvesting and conversion at high temperatures, their high tendency to diffuse and oxidize may cause a substantially reduced lifetime of devices. To address this issue, herein, we demonstrate that Ni nanoparticles individually encapsulated in a densified ceramic shell, achieved by a SiO2 coating and a subsequent densification process, possess significantly enhanced stability at high temperatures. Ni diffusion is effectively prevented at temperatures as high as 800 degrees C, and the oxidation of the Ni nanoparticles is suppressed at 500 degrees C when exposed to air. A spectrally selective absorbing film fabricated with these densified Ni@SiO2 NPs exhibits high optical absorption with reflectance <20% in the main solar radiation region, superior to that of semiconductor Si-based solar absorbing films. It also exhibits high thermal stability at 500 degrees C in air, a temperature at which thermal degradation begins for most selective solar absorbers with high-melting-point metals and metal nitrides. The Ni@SiO2 absorbing film developed in this work outperforms state-of-the-art high-temperature solar absorbers, suggesting its applicability in high-temperature solar-thermal conversion systems.

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GB/T 7714 Ding, Dawei , Liu, Kai , Fan, Qikui et al. Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption [J]. | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (7) : 3039-3045 .
MLA Ding, Dawei et al. "Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption" . | JOURNAL OF MATERIALS CHEMISTRY A 7 . 7 (2019) : 3039-3045 .
APA Ding, Dawei , Liu, Kai , Fan, Qikui , Dong, Bitao , Zhang, Yang , Yin, Yadong et al. Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption . | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (7) , 3039-3045 .
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Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries SCIE
期刊论文 | 2019 , 7 (4) , 1779-1784 | JOURNAL OF MATERIALS CHEMISTRY A
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Metal nitride materials are considered as promising candidates for next-generation lithium-ion secondary battery anode materials owing to their high electrical conductivity and attractive theoretical capacity. In this paper, we reported a synthesis method to grow ultrafine Ni3N-Co3N nanoparticles on carbon nanotubes (Ni3N-Co3N@CNTs) via a simple hydrothermal reaction and post-ammonization treatment. By virtue of such a unique structure and component, especially the abundant phase boundaries between Ni3N and Co3N, when used as anodes for lithium-ion batteries (LIBs), the resultant composites delivered reversible discharge capacity of 553.26 mA h g(-1) even after 600 cycles at a current density of 0.4 A g(-1). This reversible capacity was remarkably higher than the theoretical capacities of both Ni3N (424.3 mA h g(-1)) and Co3N (421.0 mA h g(-1)). We believe that this study will provide a new idea to design high-performance anode materials for LIBs via constructing abundant phase boundaries between different components in composites.

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GB/T 7714 Zhou, Han , Li, Zhaoyang , Wang, Ke et al. Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries [J]. | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (4) : 1779-1784 .
MLA Zhou, Han et al. "Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries" . | JOURNAL OF MATERIALS CHEMISTRY A 7 . 4 (2019) : 1779-1784 .
APA Zhou, Han , Li, Zhaoyang , Wang, Ke , Gao, Mengqiu , Ding, Shujiang . Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries . | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (4) , 1779-1784 .
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Stable Luminous Nanocomposites of Confined Mn2+-Doped Lead Halide Perovskite Nanocrystals in Mesoporous Silica Nanospheres as Orange Fluorophores SCIE
期刊论文 | 2019 , 58 (6) , 3950-3958 | INORGANIC CHEMISTRY
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Creating highly stable inorganic perovskite nanocrystals (CsPbX3, where X = Cl, Br, and I) with excellent optical performance is challenging because their optical properties depend on their ionic structure and its inherent defects. Here, we present a facile and effective synthesis using a nanoconfinement strategy to grow Mn2+-doped CsPbCl3 nanocrystals embedded in dendritic mesoporous silica nanospheres (MSNs). The resulting nanocomposite is abbreviated as Cs(Pb-x/Mn1-x)Cl-3@MSNs and can serve as the orange emitter for white light-emitting diodes (WLEDs). The MSN matrix was prepared via a templated sol gel technique as monodispersed center-radial dendritic porous particles, with a diamater of similar to 105 nm and an inner pore size of similar to 13 nm. The MSN was then utilized as the matrix to initiate the growth of Mn-doped perovskite nanocrystals (NCs). The NCs in the resulting composite have an average diameter of 8 nm and a photoluminescence quantum yield of >30%. In addition, the optical properties of the Cs(Pb-x/Mn1-x)Cl-3@MSNs can be tuned by varying the Mn2+ doping level. The resulting composites presented a significantly improved resistance to ultraviolet (UV) light, temperature, and moisture compared to that of bare Cs(Pb-0.72/Mn-0.28)Cl-3. Finally, we fabricated down-converting WLEDs by using Cs(Pb-x/Mn1-x)Cl-3@MSNs as the orange-emitting phosphor deposited onto UV-emitting chips, demonstrating their promising applications in solid-state lighting. This work provides a valuable approach to fabricating stable orange luminophores as replacements for traditional emitters in light-emitting diode devices.

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GB/T 7714 Pan, Aizhao , Wu, Youshen , Yan, Ke et al. Stable Luminous Nanocomposites of Confined Mn2+-Doped Lead Halide Perovskite Nanocrystals in Mesoporous Silica Nanospheres as Orange Fluorophores [J]. | INORGANIC CHEMISTRY , 2019 , 58 (6) : 3950-3958 .
MLA Pan, Aizhao et al. "Stable Luminous Nanocomposites of Confined Mn2+-Doped Lead Halide Perovskite Nanocrystals in Mesoporous Silica Nanospheres as Orange Fluorophores" . | INORGANIC CHEMISTRY 58 . 6 (2019) : 3950-3958 .
APA Pan, Aizhao , Wu, Youshen , Yan, Ke , Yu, Yun , Jurow, Matthew J. , Ren, Baoyi et al. Stable Luminous Nanocomposites of Confined Mn2+-Doped Lead Halide Perovskite Nanocrystals in Mesoporous Silica Nanospheres as Orange Fluorophores . | INORGANIC CHEMISTRY , 2019 , 58 (6) , 3950-3958 .
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3D ordered mesoporous TiO2@CMK-3 nanostructure for sodium-ion batteries with long-term and high-rate performance SCIE
期刊论文 | 2019 , 30 (23) | NANOTECHNOLOGY
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Sodium ion battery is abundant in resources and costs low, making it very competitive in the large-scale energy storage devices. The anatase TiO2 electrode material with insertion/extraction mechanism shows stable cycling performance, which is more in line with the technical requirements of large-scale energy storage batteries. To improve the electrical conductivity and stability of the TiO2 electrode materials, we have synthesized anatase TiO2 and CMK-3 composite. TiO2 nanoparticles were deposited on the surface of CMK-3 by hydrothermal reaction, and the anode material of the SIBs with 3D network structure was prepared. With the CMK-3, the structure stability, conductivity and reaction kinetics of TiO2@CMK-3 composite is improved. The electrochemical behavior is dominated by pseudocapacitance, which gives the material excellent high-rate performance. It delivers a reversible specific capacity of 186.3 mA h g(-1) after 100 cycles at the current density of 50 mA g(-1), 124.5 mA h g(-1) after 500 long-term cycles, meanwhile it shows an outstanding rate performance, a reversible specific capacity of 105.9 mA h g(-1) at 1600 mA g(-1), 177.3 mA h g(-1) when the current density drops to 50 mA g(-1).

Keyword :

3D network structure sodium ion batteries pseudocapacitance contributions TiO2 ordered mesoporous carbon

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GB/T 7714 Zhang, Dongyang , Liu, Limin , Zhang, Yuan et al. 3D ordered mesoporous TiO2@CMK-3 nanostructure for sodium-ion batteries with long-term and high-rate performance [J]. | NANOTECHNOLOGY , 2019 , 30 (23) .
MLA Zhang, Dongyang et al. "3D ordered mesoporous TiO2@CMK-3 nanostructure for sodium-ion batteries with long-term and high-rate performance" . | NANOTECHNOLOGY 30 . 23 (2019) .
APA Zhang, Dongyang , Liu, Limin , Zhang, Yuan , Wu, Hu , Zheng, Yuansuo , Gao, Guoxin et al. 3D ordered mesoporous TiO2@CMK-3 nanostructure for sodium-ion batteries with long-term and high-rate performance . | NANOTECHNOLOGY , 2019 , 30 (23) .
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MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage SCIE
期刊论文 | 2019 , 7 (8) , 4126-4133 | JOURNAL OF MATERIALS CHEMISTRY A
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In this study, we report a two dimensional network through the combination of CoO nanoparticles and nitrogen doped carbon nanotubes (CoO-NCNTs) derived from a lamellar coordination polymer, ([Co-II(2,3-chedc)(DABCO)(0.5)]), (2,3-chedc, cyclohexene-2,3-dicarboxylate; DABCO, 1,4-diazabicyclo [2.2.2]octane). During the pyrolysis of this two dimensional metal-organic framework (MOF), the NCNTs emerge accompanied with the catalysis of CoO nanoparticles and are connected to form two dimensional networks. The cobalt oxide particles are encapsulated and remain at the apical position of NCNTs. Due to the specific architecture and high content of CoO in the composite, it possesses great potential for lithium/sodium storage. Noticeably, high capacity and super long calendar life of 2000 cycles with only 0.0063% capacity loss per cycle is acquired for Li storage at a current density of 500 mA g(-1). In addition, it also exhibits good sodium storage performance, which delivers a high capacity of 450 mA h g(-1), and long cycling capability for 300 cycles with a capacity loss of 0.066% at a rate of 500 mA g(-1). Remarkable performance emphasizes the great potential of the two dimensional MOFs for extensive utilizations in energy storage and transfer processes.

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GB/T 7714 Pang, Yuanchao , Chen, Sheng , Xiao, Chunhui et al. MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage [J]. | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (8) : 4126-4133 .
MLA Pang, Yuanchao et al. "MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage" . | JOURNAL OF MATERIALS CHEMISTRY A 7 . 8 (2019) : 4126-4133 .
APA Pang, Yuanchao , Chen, Sheng , Xiao, Chunhui , Ma, Sude , Ding, Shujiang . MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage . | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (8) , 4126-4133 .
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Construction of ultrafine ZnSe nanoparticles on/in amorphous carbon hollow nanospheres with high-power-density sodium storage SCIE
期刊论文 | 2019 , 59 , 762-772 | NANO ENERGY
WoS CC Cited Count: 3
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Abstract :

Sodium-ion batteries (SIBs) are considered as a promising candidate to lithium-ion batteries (LIBs) owing to the inexpensive and abundant sodium reserves. However, the application of anode materials for SIBs still confront rapid capacity fading and undesirable rate capability. Here we simultaneously grow ultrafine ZnSe nanoparticles on the inner walls and the outer surface of hollow carbon nanospheres (ZnSe@HCNs), giving a unique hierarchical hybrid nanostructure that can sustain a capacity of 361.9 mAh g(-1) at 1 A g(-1) over 1000 cycles and 266.5 mAh g(-1) at 20 A g(-1). Our investigations indicate that the sodium storage mechanism of ZnSe@HCNs electrodes is a mixture of alloying and conversion reactions, where ZnSe converts to Na2Se and NaZn13 through a series of intermediate compounds. Also, a full cell is constructed from our designed ZnSe@HCNs anode and Na3V2(PO4)(3) cathode. It delivers a reversible discharge capacity of about 313.1 mAh g(-1) after 100 cycles at 0.5 A g(-1) with high Columbic efficiency over 98.2%. The outstanding sodium storage of as-prepared ZnSe@HCNs is attributed to the confinement of ZnSe structural changes both inside/outside of hollow nanospheres during the sodiation/desodiation processes. Our work offers a promising design to enable high-power-density electrodes for the various battery systems.

Keyword :

ZnSe Sodium-ion battery Full cell Hollow carbon spheres Anode

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GB/T 7714 Lu, Shiyao , Zhu, Tianxiang , Wu, Hu et al. Construction of ultrafine ZnSe nanoparticles on/in amorphous carbon hollow nanospheres with high-power-density sodium storage [J]. | NANO ENERGY , 2019 , 59 : 762-772 .
MLA Lu, Shiyao et al. "Construction of ultrafine ZnSe nanoparticles on/in amorphous carbon hollow nanospheres with high-power-density sodium storage" . | NANO ENERGY 59 (2019) : 762-772 .
APA Lu, Shiyao , Zhu, Tianxiang , Wu, Hu , Wang, Yuankun , Li, Jiao , Abdelkaderkh, Amr et al. Construction of ultrafine ZnSe nanoparticles on/in amorphous carbon hollow nanospheres with high-power-density sodium storage . | NANO ENERGY , 2019 , 59 , 762-772 .
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In-situ fabrication of transition-metal-doped TiO2 nanofiber/nanosheet structure for high-performance Li storage SCIE
期刊论文 | 2019 , 787 , 1110-1119 | JOURNAL OF ALLOYS AND COMPOUNDS
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Constructing special nanostructures and ion doping are effective strategies to improve the intrinsic Li storage performance of anode materials in lithium ion batteries (LIBs). Various transition-metal-doped hierarchical TiO2 nanofiber/nanosheet structure (HTFSs) were in-situ fabricated in this work by the electrospinning followed by a SiO2-assisted alkali-hydrothermal method, aiming to further explore the potential anode capacity of TiO2. Firstly, Mn-doped HTFSs (Mn-HTFSs) with different Mn2+ doping amounts (0, 10, 15 and 20 wt%) were studied in detail as representative. Their morphologies, components, structures and pore properties were obtained and analyzed by different characterization techniques. Compared with the traditional electrospun TiO2 fibers and other Mn-HTFSs, 15 wt% Mn2+ doped Mn-HTFSs as the anode material for LIBs exhibited the highest reversible discharge capacity of 262.2 mA h g(-1) at the current density of 0.4 A g(-1) after 1200 cycles, with nearly a 100% capacity retention between 20 and 1200 cycles. The excellent performance of 15 wt% Mn2+ doped Mn-HTFSs can be convincingly attributed to its in-situ formed hierarchical nanofiber/nanosheet structure, high surface area and especially appropriate amount of Mn2+ doping. Furthermore, Mn2+ doped Mn-HTFSs also delivered a better capacity performance than other transition-metal-doped HTFSs (A-HTFSs (A = Ni, Co, Zn and Cu)) fabricated by the similar method, suggesting its promising application prospect in practical LIBs. (C) 2019 Elsevier B.V. All rights reserved.

Keyword :

Transition metal doping Electrospinning Nanosheet Lithium-ion batteries Nanofibers

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GB/T 7714 Wang, Jianan , Yang, Guorui , Wang, Ling et al. In-situ fabrication of transition-metal-doped TiO2 nanofiber/nanosheet structure for high-performance Li storage [J]. | JOURNAL OF ALLOYS AND COMPOUNDS , 2019 , 787 : 1110-1119 .
MLA Wang, Jianan et al. "In-situ fabrication of transition-metal-doped TiO2 nanofiber/nanosheet structure for high-performance Li storage" . | JOURNAL OF ALLOYS AND COMPOUNDS 787 (2019) : 1110-1119 .
APA Wang, Jianan , Yang, Guorui , Wang, Ling , Wang, Silan , Yan, Wei , Ding, Shujiang . In-situ fabrication of transition-metal-doped TiO2 nanofiber/nanosheet structure for high-performance Li storage . | JOURNAL OF ALLOYS AND COMPOUNDS , 2019 , 787 , 1110-1119 .
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NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst EI Scopus SCIE
期刊论文 | 2019 , 294 , 38-45 | Electrochimica Acta
WoS CC Cited Count: 1 SCOPUS Cited Count: 2
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© 2018 Elsevier Ltd Exploiting high efficient non-noble metal catalysts with low-cost and good stability for oxygen reduction reaction (ORR) is vital for fuel cells and metal-air batteries. In this work, we successfully constructed a novel nanosheets-shaped NiCoO2 hierarchical structure supported on CMK-3 support (i.e., NiCoO2@CMK-3 composite) via a facile hydrothermal method. Electrochemical characterization results reveal that the as-prepared NiCoO2@CMK-3 composite exhibits remarkable ORR electrocatalytic activity with a positive peak potential of 0.81 V (vs. RHE), an onset potential of 0.90 V (vs. RHE), a high current density of 4.10 mA cm−2 at 0.4 V, and a nearly four-electron reduction pathway, which are comparable to the state-of-the-art Pt/C catalyst with the same mass. In addition, the NiCoO2@CMK-3 composite possesses excellent methanol-tolerance and electrochemical stability, which are better than Pt/C. The outstanding performance confirms the NiCoO2@CMK-3 composite as a promising efficient ORR catalyst in fuel cells and metal-air batteries.

Keyword :

Electrocatalyst Fuel cells NiCoO2@CMK-3 composite Oxygen reduction reaction

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GB/T 7714 Sun, Yao , Li, Fei , Shen, Zichao et al. NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst [J]. | Electrochimica Acta , 2019 , 294 : 38-45 .
MLA Sun, Yao et al. "NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst" . | Electrochimica Acta 294 (2019) : 38-45 .
APA Sun, Yao , Li, Fei , Shen, Zichao , Li, Yabei , Lang, Jinxin , Li, Weimin et al. NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst . | Electrochimica Acta , 2019 , 294 , 38-45 .
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Enhanced Sulfur Transformation by Multifunctional FeS2/FeS/S Composites for High-Volumetric Capacity Cathodes in Lithium-Sulfur Batteries SCIE
期刊论文 | 2019 , 6 (6) | ADVANCED SCIENCE
WoS CC Cited Count: 3
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Lithium-sulfur batteries are currently being explored as promising advanced energy storage systems due to the high theoretical specific capacity of sulfur. However, achieving a scalable synthesis for the sulfur electrode material whilst maintaining a high volumetric energy density remains a serious challenge. Here, a continuous ball-milling route is devised for synthesizing multifunctional FeS2/FeS/S composites for use as high tap density electrodes. These composites demonstrate a maximum reversible capacity of 1044.7 mAh g(-1) and a peak volumetric capacity of 2131.1 Ah L-1 after 30 cycles. The binding direction is also considered here for the first time between dissolved lithium polysulfides (LiPSs) and host materials (FeS2 and FeS in this work) as determined by density functional theory calculations. It is concluded that if only one lithium atom of the polysulfide bonds with the sulfur atoms of FeS2 or FeS, then any chemical interaction between these species is weak or negligible. In addition, FeS2 is shown to have a strong catalytic effect on the reduction reactions of LiPSs. This work demonstrates the limitations of a strategy based on chemical interactions to improve cycling stability and offers new insights into the development of high tap density and high-performance sulfur-based electrodes.

Keyword :

lithium-sulfur batteries FeS2/FeS/S composites volumetric energy density density functional theory (DFT) calculations catalytic effect

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GB/T 7714 Xi, Kai , He, Deqing , Harris, Chris et al. Enhanced Sulfur Transformation by Multifunctional FeS2/FeS/S Composites for High-Volumetric Capacity Cathodes in Lithium-Sulfur Batteries [J]. | ADVANCED SCIENCE , 2019 , 6 (6) .
MLA Xi, Kai et al. "Enhanced Sulfur Transformation by Multifunctional FeS2/FeS/S Composites for High-Volumetric Capacity Cathodes in Lithium-Sulfur Batteries" . | ADVANCED SCIENCE 6 . 6 (2019) .
APA Xi, Kai , He, Deqing , Harris, Chris , Wang, Yuankun , Lai, Chao , Li, Huanglong et al. Enhanced Sulfur Transformation by Multifunctional FeS2/FeS/S Composites for High-Volumetric Capacity Cathodes in Lithium-Sulfur Batteries . | ADVANCED SCIENCE , 2019 , 6 (6) .
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