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NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst EI Scopus SCIE
期刊论文 | 2019 , 294 , 38-45 | Electrochimica Acta
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Abstract :

© 2018 Elsevier Ltd Exploiting high efficient non-noble metal catalysts with low-cost and good stability for oxygen reduction reaction (ORR) is vital for fuel cells and metal-air batteries. In this work, we successfully constructed a novel nanosheets-shaped NiCoO2 hierarchical structure supported on CMK-3 support (i.e., NiCoO2@CMK-3 composite) via a facile hydrothermal method. Electrochemical characterization results reveal that the as-prepared NiCoO2@CMK-3 composite exhibits remarkable ORR electrocatalytic activity with a positive peak potential of 0.81 V (vs. RHE), an onset potential of 0.90 V (vs. RHE), a high current density of 4.10 mA cm−2 at 0.4 V, and a nearly four-electron reduction pathway, which are comparable to the state-of-the-art Pt/C catalyst with the same mass. In addition, the NiCoO2@CMK-3 composite possesses excellent methanol-tolerance and electrochemical stability, which are better than Pt/C. The outstanding performance confirms the NiCoO2@CMK-3 composite as a promising efficient ORR catalyst in fuel cells and metal-air batteries.

Keyword :

Electrocatalyst Fuel cells NiCoO2@CMK-3 composite Oxygen reduction reaction

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GB/T 7714 Sun, Yao , Li, Fei , Shen, Zichao et al. NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst [J]. | Electrochimica Acta , 2019 , 294 : 38-45 .
MLA Sun, Yao et al. "NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst" . | Electrochimica Acta 294 (2019) : 38-45 .
APA Sun, Yao , Li, Fei , Shen, Zichao , Li, Yabei , Lang, Jinxin , Li, Weimin et al. NiCoO2@CMK-3 composite with nanosheets-mesoporous structure as an efficient oxygen reduction catalyst . | Electrochimica Acta , 2019 , 294 , 38-45 .
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Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption SCIE
期刊论文 | 2019 , 7 (7) , 3039-3045 | JOURNAL OF MATERIALS CHEMISTRY A
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Abstract :

While non-noble transition metal nanoparticles are widely explored in the field of solar energy harvesting and conversion at high temperatures, their high tendency to diffuse and oxidize may cause a substantially reduced lifetime of devices. To address this issue, herein, we demonstrate that Ni nanoparticles individually encapsulated in a densified ceramic shell, achieved by a SiO2 coating and a subsequent densification process, possess significantly enhanced stability at high temperatures. Ni diffusion is effectively prevented at temperatures as high as 800 degrees C, and the oxidation of the Ni nanoparticles is suppressed at 500 degrees C when exposed to air. A spectrally selective absorbing film fabricated with these densified Ni@SiO2 NPs exhibits high optical absorption with reflectance <20% in the main solar radiation region, superior to that of semiconductor Si-based solar absorbing films. It also exhibits high thermal stability at 500 degrees C in air, a temperature at which thermal degradation begins for most selective solar absorbers with high-melting-point metals and metal nitrides. The Ni@SiO2 absorbing film developed in this work outperforms state-of-the-art high-temperature solar absorbers, suggesting its applicability in high-temperature solar-thermal conversion systems.

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GB/T 7714 Ding, Dawei , Liu, Kai , Fan, Qikui et al. Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption [J]. | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (7) : 3039-3045 .
MLA Ding, Dawei et al. "Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption" . | JOURNAL OF MATERIALS CHEMISTRY A 7 . 7 (2019) : 3039-3045 .
APA Ding, Dawei , Liu, Kai , Fan, Qikui , Dong, Bitao , Zhang, Yang , Yin, Yadong et al. Nickel nanoparticles individually encapsulated in densified ceramic shells for thermally stable solar energy absorption . | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (7) , 3039-3045 .
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Ultrathin NiFe-layered double hydroxide decorated NiCo2O4 arrays with enhanced performance for supercapacitors EI Scopus SCIE
期刊论文 | 2019 , 465 , 929-936 | Applied Surface Science
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Abstract :

Designing and synthesizing core/shell nanostructures materials as binder-free electrodes is an effective strategy to enhance the electrochemical performance of supercapacitors. In this work, the hierarchical NiCo2O4@NiFe-layered double hydroxide core/shell arrays are successfully constructed via a stepwise hydrothermally grow method and investigated for application in supercapacitors. With the assistance of the hierarchical core/shell structures and the synergetic effect between NiCo2O4 and NiFe-layered double hydroxide nanosheets, the hybrid electrode discloses significant melioration in property, including the improvement in number of the electrochemically active sites and short transport path lengths for both electrons and ions. Thus, the core/shell electrode exhibits remarkable electrochemical performance, such as a high areal capacity (12.3 F cm−2) and good cycling stability (83.1% capacitance retention after 2000 cycles). Our trials testify that the hierarchical NiCo2O4@NiFe-layered double hydroxide core/shell nanowire arrays are advantageous for potential applications in energy storage devices. © 2018

Keyword :

Capacitance retention Core/shell Core/shell nanowire arrays Electrochemical energy storage Electrochemical performance Layered double hydroxide nanosheets Layered double hydroxides Nanostructures materials

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GB/T 7714 Gao, Haixing , Cao, Yang , Chen, Yong et al. Ultrathin NiFe-layered double hydroxide decorated NiCo2O4 arrays with enhanced performance for supercapacitors [J]. | Applied Surface Science , 2019 , 465 : 929-936 .
MLA Gao, Haixing et al. "Ultrathin NiFe-layered double hydroxide decorated NiCo2O4 arrays with enhanced performance for supercapacitors" . | Applied Surface Science 465 (2019) : 929-936 .
APA Gao, Haixing , Cao, Yang , Chen, Yong , Liu, Zheng , Guo, Mingliang , Ding, Shujiang et al. Ultrathin NiFe-layered double hydroxide decorated NiCo2O4 arrays with enhanced performance for supercapacitors . | Applied Surface Science , 2019 , 465 , 929-936 .
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Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin. PubMed SCIE
期刊论文 | 2019 , 45 (2) , 273-281 | Drug development and industrial pharmacy
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The aim of this work is to develop curcumin-loaded hollow mesoporous silica microspheres (HMSMs@curcumin) to improve the poor oral bioavailability of curcumin. Hollow mesoporous silica microspheres (HMSMs) were synthesized in facile route using a hard template. HMSMs and HMSMs@curcumin were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), nitrogen adsorption/desorption measurements, differential scanning calorimetry (DSC), Fourier transform infrared (FTIR) and X-ray diffraction (XRD). In addition, to demonstrate the potential application of the HMSMs@curcumin, cytotoxicity, in vitro release behavior and in vivo pharmacokinetics of curcumin loaded in these HMSMs were investigated by using of Caco-2 cells and Sprague-Dawley (SD) rats, respectively. These mono-dispersed HMSMs exhibited high drug loading ratio and encapsulation efficiency due to the mesoporous shell and hollow core. The excellent characteristics of HMSMs such as mono-dispersed morphology, smooth surface, uniform, ordered and size-narrowing mesopores resulted in a good in vitro release profile of curcumin from HMSMs@curcumin. Moreover, an impressive improvement in the oral absorption of curcumin and prolonged systemic circulation time were achieved in the in vivo animal studies. In addition, the good biocompatibility of developed HMSMs with Caco-2 cells was confirmed based on the in vitro cytotoxicity assay. In conclusion, this system demonstrated a great potential for efficiently delivery of curcumin in vitro and in vivo, suggesting a good prospect for its application in clinic for therapeutic drug delivery in future.

Keyword :

Cytotoxicity Hollow mesoporous silica microspheres (HMSMs) Curcumin In vivo drug delivery In vitro drug release

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GB/T 7714 Gao Yang , Ding Shujiang , Huang Xiaoyan et al. Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin. [J]. | Drug development and industrial pharmacy , 2019 , 45 (2) : 273-281 .
MLA Gao Yang et al. "Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin." . | Drug development and industrial pharmacy 45 . 2 (2019) : 273-281 .
APA Gao Yang , Ding Shujiang , Huang Xiaoyan , Fan Zhaoyang , Sun Jianmei , Hai Yang et al. Development and evaluation of hollow mesoporous silica microspheres bearing on enhanced oral delivery of curcumin. . | Drug development and industrial pharmacy , 2019 , 45 (2) , 273-281 .
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Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries SCIE
期刊论文 | 2019 , 7 (4) , 1779-1784 | JOURNAL OF MATERIALS CHEMISTRY A
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Metal nitride materials are considered as promising candidates for next-generation lithium-ion secondary battery anode materials owing to their high electrical conductivity and attractive theoretical capacity. In this paper, we reported a synthesis method to grow ultrafine Ni3N-Co3N nanoparticles on carbon nanotubes (Ni3N-Co3N@CNTs) via a simple hydrothermal reaction and post-ammonization treatment. By virtue of such a unique structure and component, especially the abundant phase boundaries between Ni3N and Co3N, when used as anodes for lithium-ion batteries (LIBs), the resultant composites delivered reversible discharge capacity of 553.26 mA h g(-1) even after 600 cycles at a current density of 0.4 A g(-1). This reversible capacity was remarkably higher than the theoretical capacities of both Ni3N (424.3 mA h g(-1)) and Co3N (421.0 mA h g(-1)). We believe that this study will provide a new idea to design high-performance anode materials for LIBs via constructing abundant phase boundaries between different components in composites.

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GB/T 7714 Zhou, Han , Li, Zhaoyang , Wang, Ke et al. Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries [J]. | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (4) : 1779-1784 .
MLA Zhou, Han et al. "Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries" . | JOURNAL OF MATERIALS CHEMISTRY A 7 . 4 (2019) : 1779-1784 .
APA Zhou, Han , Li, Zhaoyang , Wang, Ke , Gao, Mengqiu , Ding, Shujiang . Phase boundary- enhanced Ni3N-Co3N@ CNT composite materials for lithium- ion batteries . | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (4) , 1779-1784 .
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MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage SCIE
期刊论文 | 2019 , 7 (8) , 4126-4133 | JOURNAL OF MATERIALS CHEMISTRY A
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In this study, we report a two dimensional network through the combination of CoO nanoparticles and nitrogen doped carbon nanotubes (CoO-NCNTs) derived from a lamellar coordination polymer, ([Co-II(2,3-chedc)(DABCO)(0.5)]), (2,3-chedc, cyclohexene-2,3-dicarboxylate; DABCO, 1,4-diazabicyclo [2.2.2]octane). During the pyrolysis of this two dimensional metal-organic framework (MOF), the NCNTs emerge accompanied with the catalysis of CoO nanoparticles and are connected to form two dimensional networks. The cobalt oxide particles are encapsulated and remain at the apical position of NCNTs. Due to the specific architecture and high content of CoO in the composite, it possesses great potential for lithium/sodium storage. Noticeably, high capacity and super long calendar life of 2000 cycles with only 0.0063% capacity loss per cycle is acquired for Li storage at a current density of 500 mA g(-1). In addition, it also exhibits good sodium storage performance, which delivers a high capacity of 450 mA h g(-1), and long cycling capability for 300 cycles with a capacity loss of 0.066% at a rate of 500 mA g(-1). Remarkable performance emphasizes the great potential of the two dimensional MOFs for extensive utilizations in energy storage and transfer processes.

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GB/T 7714 Pang, Yuanchao , Chen, Sheng , Xiao, Chunhui et al. MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage [J]. | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (8) : 4126-4133 .
MLA Pang, Yuanchao et al. "MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage" . | JOURNAL OF MATERIALS CHEMISTRY A 7 . 8 (2019) : 4126-4133 .
APA Pang, Yuanchao , Chen, Sheng , Xiao, Chunhui , Ma, Sude , Ding, Shujiang . MOF derived CoO-NCNTs two-dimensional networks for durable lithium and sodium storage . | JOURNAL OF MATERIALS CHEMISTRY A , 2019 , 7 (8) , 4126-4133 .
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PEO-based polymer electrolytes in lithium ion batteries EI CSCD
期刊论文 | 2018 , 63 (22) , 2280-2295 | Kexue Tongbao/Chinese Science Bulletin
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Abstract :

Currently, electrolytes used in lithium-ion batteries are flammable and leaky, causing safety problems when used under high temperatures or extreme conditions. Solid electrolytes can fundamentally avoid the occurrence of such issues, at the same time, it can significantly increase the energy density of solid state lithium batteries. Solid electrolytes are classified into inorganic solid electrolytes and solid polymer electrolytes. Although inorganic solid electrolytes have the high mechanical strength and room temperature ionic conductivity, it has poor flexibility and complicated preparation process. In contrast, solid polymer electrolyte has good elasticity and good interface contact, which can overcome many disadvantages of the inorganic solid electrolyte. Among them, polyethylene oxide (PEO) is first proposed as a polymer electrolyte. Due to its excellent mechanical properties, electrochemical stability and thermal stability, it has been a hot topic for polymer solid electrolytes for decades. However, its low room temperature ionic conductivity limits practical application. Given the problems existing in PEO-based polymer electrolytes, several methods for improving ionic conductivity have been proposed. The primary methods include plasticization, the organic-inorganic composite, and polymer blending. Comparing these methods, it can be seen that adding plasticizers to the polymer can effectively increase the conductivity of the electrolyte, but at the same time it will cause a decrease in the mechanical properties, and the safety issues limit its application in lithium-ion batteries. Inorganic fillers can balance the problems of ionic conductivity and mechanical properties, but the construction of a good filler-polymer dispersion system is complicated in preparing such composite electrolytes, design a new type of multi-dimensional the ion transport network also face tremendous challenges. Undoubtedly, in the future research, inorganic fillers will be the dominant means in the modification of composite electrolytes. Compared with the former two modification methods, polymer blending is easy to operate and friendly to industry, but low ionic conductivity at room temperature still exist. To give full play to the advantages of polymer blending, using it as an auxiliary means to improve the performance of composite electrolytes will be the primary development direction of such modification methods. PEO is the most widely studied polymer electrolyte. Even though a large number of modification methods have emerged in its development history, the ionic conductivity at room temperature is still limited to a relatively low level. To meet the needs of the application in lithium-ion batteries, a high operating temperature (50-70℃) is still needed, the biggest problem remains exist. To solve the problems in polymer solid electrolytes, the research directions in the future may mainly focus on: Expanding the modification method of PEO to other polymer electrolyte host materials, broadening the scope of research, and finding the available polymer electrolytes at room temperature. Concerned about the preparation of ultra-thin polymer electrolytes, reducing the ion transmission path to increase the transmission efficiency of lithium ions between positive and negative electrodes. Effectively combines inorganic solid electrolytes and solid polymer electrolytes to give full play to their advantages. In addition, exploring the effect of inorganic filler morphology on the conductivity of the composite electrolyte will also deserve attention. Many one-dimensional, two-dimensional materials can build ion transport networks so that lithium ions can travel rapidly along the path. With the deepening of research, it is expected that PEO-based polymer electrolytes may replace liquid electrolytes and become an essential cornerstone for building the next generation of safe and reliable lithium-ion batteries. © 2018, Science Press. All right reserved.

Keyword :

All-solid state batteries Electrochemical stabilities High operating temperature Inorganic solid electrolytes Organic-inorganic composite Peo-based polymer electrolytes Solid polymer electrolytes Solid-state lithium batteries

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GB/T 7714 Sun, Zongjie , Ding, Shujiang . PEO-based polymer electrolytes in lithium ion batteries [J]. | Kexue Tongbao/Chinese Science Bulletin , 2018 , 63 (22) : 2280-2295 .
MLA Sun, Zongjie et al. "PEO-based polymer electrolytes in lithium ion batteries" . | Kexue Tongbao/Chinese Science Bulletin 63 . 22 (2018) : 2280-2295 .
APA Sun, Zongjie , Ding, Shujiang . PEO-based polymer electrolytes in lithium ion batteries . | Kexue Tongbao/Chinese Science Bulletin , 2018 , 63 (22) , 2280-2295 .
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Mesoporous TiO2 nanosheets anchored on graphene for ultra long life Na-ion batteries EI SCIE PubMed Scopus
期刊论文 | 2018 , 29 (22) | NANOTECHNOLOGY
WoS CC Cited Count: 6 SCOPUS Cited Count: 6
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Sodium-ion batteries, which have a similar electrochemical reaction mechanism to lithium-ion batteries, have been considered as one of the most potential lithium-ion battery alternatives due to the rich reserves of sodium. However, it is very hard to find appropriate electrode materials imputing the large radius of sodium-ion. TiO2 is particularly interesting as anodes for sodium-ion batteries due to their reasonable operation voltage, cost, and nontoxicity. To obtain a better electrochemical property, mesoporous TiO2 nanosheets (NSs)/reduced graphene oxide (rGO) composites have been synthesized via a scalable hydrothermal-solvothermal method with a subsequent calcination process. Benefitting from unique structure design, TiO2 NSs@rGO exhibits a superior cycle stability (90 mAh g(-1) after 10 000 cycles at a high current rate of 20 C) and satisfactory rate performance (97.3 mAh g(-1) at 25 C). To our knowledge, such ultra long cycle life has not previously been reported.

Keyword :

nanosheets ultra long life graphene sodium-ion batteries anatase TiO2

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GB/T 7714 Zhang, Ruifang , Wang, Yuankun , Zhou, Han et al. Mesoporous TiO2 nanosheets anchored on graphene for ultra long life Na-ion batteries [J]. | NANOTECHNOLOGY , 2018 , 29 (22) .
MLA Zhang, Ruifang et al. "Mesoporous TiO2 nanosheets anchored on graphene for ultra long life Na-ion batteries" . | NANOTECHNOLOGY 29 . 22 (2018) .
APA Zhang, Ruifang , Wang, Yuankun , Zhou, Han , Lang, Jinxin , Xu, Jingjing , Xiang, Yang et al. Mesoporous TiO2 nanosheets anchored on graphene for ultra long life Na-ion batteries . | NANOTECHNOLOGY , 2018 , 29 (22) .
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Ultrafast microwave-assisted synthesis of nitrogen-doped carbons as electrocatalysts for oxygen reduction reaction SCIE PubMed
期刊论文 | 2018 , 29 (30) | NANOTECHNOLOGY
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A facile and ultrafast microwave-assisted thermolysis approach has been adopted to synthesize hierarchical nitrogen-doped carbon within a very short time. The precursor PANI@ carbon felt composite was pyrolyzed in microwave oven for different time (10, 20, 30, 40, 50 s) and denoted as NC-X (X = 10, 20, 30, 40, 50). As for NC-30, nitrogen-doping content is obtained up to 3.62 at% with striking enrichment of pyridinic N as high as 45% of the total nitrogen content. Raman analysis indicates the extent graphitization level for the resultant NC-30 and the relative intensity I-D/I-G was 1.26. High nitrogen-doping content and graphitization level provide effective active sites and efficient electron transfer channel. The resultant NC-30 exhibits pronounced ORR activity with an onset potential of 0.94 V (versus RHE), half-wave potential of 0.80 V and diffusion limiting current density of -5.23 mA cm(-2), comparable to those of the commercial Pt/ C. It also shows enhanced stability with current retention of 98.3% over 7.5 h as well as superior tolerance against methanol. The simple preparation and excellent ORR performance of NC-30 suggest its promising practical application.

Keyword :

oxygen reduction reaction PANI@carbon felt composites electrocatalyst microwave nitrogen-doped carbons

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GB/T 7714 Xu, Jingjing , Zhang, Ruifang , Lu, Shiyao et al. Ultrafast microwave-assisted synthesis of nitrogen-doped carbons as electrocatalysts for oxygen reduction reaction [J]. | NANOTECHNOLOGY , 2018 , 29 (30) .
MLA Xu, Jingjing et al. "Ultrafast microwave-assisted synthesis of nitrogen-doped carbons as electrocatalysts for oxygen reduction reaction" . | NANOTECHNOLOGY 29 . 30 (2018) .
APA Xu, Jingjing , Zhang, Ruifang , Lu, Shiyao , Liu, Huan , Li, Zhaoyang , Zhang, Xinyu et al. Ultrafast microwave-assisted synthesis of nitrogen-doped carbons as electrocatalysts for oxygen reduction reaction . | NANOTECHNOLOGY , 2018 , 29 (30) .
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Au nanoparticle-decorated NiCo2O4 nanoflower with enhanced electrocatalytic activity toward methanol oxidation EI SCIE Scopus
期刊论文 | 2018 , 732 , 460-469 | JOURNAL OF ALLOYS AND COMPOUNDS
WoS CC Cited Count: 2
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The performance of direct methanol fuel cells hinges on the activity of the catalyst. To enhance the electro-catalytic activity, a flower-like nanostructure assembled from thin Au/NiCo2O4 nanosheet is synthesized via a microwave process combined with deposition-reduction method, where the Au nanoparticles are well dispersed on the surface of the NiCo2O4 nanosheet. The Au/NiCo2O4 composite nanoflower is successfully applied in the electro-catalytic oxidation of methanol and its electro-catalytic performance is investigated by cyclic voltammetry, chronoamperometry and electrochemical impedance spectroscopy, which exhibits excellent electro-catalytic qualities towards methanol electro-oxidation in alkaline medium, including low onset potential (0.31 V), high current densities (135.9 mA cm(-2)) at 0.60 V (vs. SCE), and desirable electro-oxidation stability (94%) after 500 cycles. The activity of NiCo2O4 is significantly enhanced by a small amount of Au for methanol electro-oxidation. Au, a highly electronegative metal, acted as an electron adsorbate, stimulates the generation and stabilization of Co4+ and Ni3+ cations as the active centers for methanol oxidation reactions. (C) 2017 Elsevier B.V. All rights reserved.

Keyword :

Microwave synthesis Kinetics Catalyst Nickel-cobaltite

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GB/T 7714 Gao, Haixing , Cao, Yang , Chen, Yong et al. Au nanoparticle-decorated NiCo2O4 nanoflower with enhanced electrocatalytic activity toward methanol oxidation [J]. | JOURNAL OF ALLOYS AND COMPOUNDS , 2018 , 732 : 460-469 .
MLA Gao, Haixing et al. "Au nanoparticle-decorated NiCo2O4 nanoflower with enhanced electrocatalytic activity toward methanol oxidation" . | JOURNAL OF ALLOYS AND COMPOUNDS 732 (2018) : 460-469 .
APA Gao, Haixing , Cao, Yang , Chen, Yong , Lai, Xiaoyong , Ding, Shujiang , Tu, Jinchun et al. Au nanoparticle-decorated NiCo2O4 nanoflower with enhanced electrocatalytic activity toward methanol oxidation . | JOURNAL OF ALLOYS AND COMPOUNDS , 2018 , 732 , 460-469 .
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