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Mn-based layered oxide microspheres assembled by ultrathin nanosheets as cathode material for potassium-ion batteries EI Scopus SCIE
期刊论文 | 2019 , 293 , 299-306 | Electrochimica Acta
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Abstract :

© 2018 Elsevier Ltd Potassium-ion batteries (KIBs) are regarded as potentially promising large-scale energy storage (EES) systems due to the close redox potential to lithium, the rich reserve and low cost of potassium resources. Nevertheless, the larger ionic radius of K-ion makes cathode materials for KIBs be a difficult issue. Herein, we construct Mn-based layered oxide (K0.32MnO2) microsphere, self-assembled by ultrathin nanosheets, as potential cathode electrode for nonaqueous KIBs, which delivers a reversible discharge capacity of 95.1 mAh·g−1 at 10 mA g−1. It is demonstrated that K0.32MnO2 undergoes a simple solid solution reaction mechanism for K-ions deintercalation/intercalation during the initial charge-discharge process, which is not like complex multiple processes accompanied by phase transition for Mn-based layered oxide particles. Ex situ measurements reveal that K0.32MnO2 nanosheets can provide outstanding morphology and structure stability, as well as fast electrochemical kinetics upon cycling, thus high rate capacity, improved cycling lifetime and voltage stability at low and high rates can be obtained. We also verify the practical feasibility of K-ion full cell with commercial super P carbon black anode. This novel work illuminates the electrochemical mechanism for K-ions storage in depth, which may push the study on layered oxide cathodes and accelerate the development of KIBs.

Keyword :

Cathode material Mn-based layered oxide Nonaqueous electrolyte Potassium-ion battery Solid solution process

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GB/T 7714 Chong, Shaokun , Wu, Yifang , Chen, Yuanzhen et al. Mn-based layered oxide microspheres assembled by ultrathin nanosheets as cathode material for potassium-ion batteries [J]. | Electrochimica Acta , 2019 , 293 : 299-306 .
MLA Chong, Shaokun et al. "Mn-based layered oxide microspheres assembled by ultrathin nanosheets as cathode material for potassium-ion batteries" . | Electrochimica Acta 293 (2019) : 299-306 .
APA Chong, Shaokun , Wu, Yifang , Chen, Yuanzhen , Guo, Shengwu , Tai, Zige , Shu, Chengyong et al. Mn-based layered oxide microspheres assembled by ultrathin nanosheets as cathode material for potassium-ion batteries . | Electrochimica Acta , 2019 , 293 , 299-306 .
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Effect of grain refinement on high-carbon martensite transformation and its mechanical properties EI SCIE Scopus
期刊论文 | 2018 , 726 , 342-349 | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
WoS CC Cited Count: 2 SCOPUS Cited Count: 2
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Abstract :

In this paper, the grain size effect on martensite transformation and its mechanical properties were investigated in two high-carbon steels. The results show that grain refinement can induce a phase transformation of high carbon martensite substructure from twin to dislocations. When grains are refined to smaller than 4 mu m, no twin could be observed, instead, full dislocation substructure is obtained. And the martensite substructure transition results in an enhancement in mechanical properties, an ultrahigh tensile strength of 2.28 GPa and a significant elongation of 6.8% are obtained in the 0.61 wt%C steel. A model based on the relationship between dislocation slip stress (tau(S)) and twin shear stress (tau(T)) with grain size (d) is developed to explain the above phase transformation phenomenon. The tau(T) is proportional to d(-1) and tau(S) is proportional to d(-1/2), both of which increase with reducing grain size, but tau(T) is more sensitive to grain size. Therefore, a critical grain size (d(c)) is obtained, at which the stresses for twining and for dislocation gliding are equal, lower than this value (i.e. grain is finer), the stress for twin is higher than that for dislocation gliding, so dislocation slip becomes main deformation process in martensite transformation. The theoretically calculated d(c) is about 2.7-7.6 mu m, which is in good agreement with the experimental results. These findings may provide a new way to design ultra-high strength and high ductility steels.

Keyword :

Martensitic phase transformation High-carbon steel Dislocation structure Twinning Mechanical property

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GB/T 7714 Sun, Junjie , Jiang, Tao , Wang, Yingjun et al. Effect of grain refinement on high-carbon martensite transformation and its mechanical properties [J]. | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2018 , 726 : 342-349 .
MLA Sun, Junjie et al. "Effect of grain refinement on high-carbon martensite transformation and its mechanical properties" . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING 726 (2018) : 342-349 .
APA Sun, Junjie , Jiang, Tao , Wang, Yingjun , Guo, Shengwu , Liu, Yongning . Effect of grain refinement on high-carbon martensite transformation and its mechanical properties . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2018 , 726 , 342-349 .
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Cryptomelane-type MnO2/carbon nanotube hybrids as bifunctional electrode material for high capacity potassium-ion full batteries EI SCIE Scopus
期刊论文 | 2018 , 54 , 106-115 | Nano Energy
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Abstract :

Potassium-ion batteries (PIBs) have been receiving a great deal of attention owing to abundant and cost-effective potassium resources. However, the key issue is to explore suitable electrode materials for accommodating the large size K-ions reversibly. In this report, K1.06Mn8O16/CNT hybrids are systematically studied for the first time as bifunctional PIBs-electrodes, in which Mn-ions play as the redox center. As the cathode, it exhibits excellent electrochemical kinetics and reversibility, as well as highly structure stability. The cathode displays an unprecedented capacity of 309.4 mA h g−1 at 20 mA g−1 with the energy density of 733.3 Wh kg−1 and outstanding rate performance (187.1 mA h g−1 at 500 mA g−1). In addition, the high capacity of 636.6 mA h g−1 at 20 mA g−1, ultra-long cycling lifespan over 500 cycles and remarkable rate capability can also be acquired when the material was tested as the anode. The extraordinary electrochemical properties are ascribed to the well-developed conductive network and robust microstructure stability. Meanwhile, the symmetrical K-ions full cell exhibits high discharge capacity of 241.0 mA h g−1 at 100 mA g−1. This work reveals the K-ions storage mechanism in cryptomelane bifunctional electrodes in depth and the fundamental understanding help us open up a new direction for PIBs. © 2018 Elsevier Ltd

Keyword :

Bifunctional electrodes Conductive networks Cryptomelane Discharge capacities Electrochemical kinetics High capacity Microstructure stability Potassium ions

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GB/T 7714 Chong, Shaokun , Wu, Yifang , Liu, Chaofeng et al. Cryptomelane-type MnO2/carbon nanotube hybrids as bifunctional electrode material for high capacity potassium-ion full batteries [J]. | Nano Energy , 2018 , 54 : 106-115 .
MLA Chong, Shaokun et al. "Cryptomelane-type MnO2/carbon nanotube hybrids as bifunctional electrode material for high capacity potassium-ion full batteries" . | Nano Energy 54 (2018) : 106-115 .
APA Chong, Shaokun , Wu, Yifang , Liu, Chaofeng , Chen, Yuanzhen , Guo, Shengwu , Liu, Yongning et al. Cryptomelane-type MnO2/carbon nanotube hybrids as bifunctional electrode material for high capacity potassium-ion full batteries . | Nano Energy , 2018 , 54 , 106-115 .
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Ultrafine grained dual-phase martensite/ferrite steel strengthened and toughened by lamella structure EI SCIE Scopus
期刊论文 | 2018 , 734 , 311-317 | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
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Abstract :

Grain refinement is one of the most effective methods for strengthening steels, but grain refinement to 1 pm or less deteriorates the ductility considerably. To evade the strength-ductility trade-off, a lamellar-structured (LS) ultrafine-grained (UFG) dual-phase (DP) ferrite/martensite (F/M) steel was produced by warm rolling an intercritical annealed low-carbon martensite and subsequent air cooling in this paper. The microstructure is similar to a short fiber reinforced composite, and the highest strength (1432 +/- 15 MPa) combined with a decent ductility (16.5 +/- 0.5% elongation) is achieved in DP steel. Compared with conventional equiaxed coarse grained (CG) and UFG DP counterparts, the LS martensite in UFG DP steel can produce extra strengthening effect and is also beneficial to ductility. And the short fiber theory can predict the strength very well.

Keyword :

Dual phases Lamella structure Mechanical properties Steel Ultrafine grained microstructure

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GB/T 7714 Sun, Junjie , Jiang, Tao , Wang, Yingjun et al. Ultrafine grained dual-phase martensite/ferrite steel strengthened and toughened by lamella structure [J]. | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2018 , 734 : 311-317 .
MLA Sun, Junjie et al. "Ultrafine grained dual-phase martensite/ferrite steel strengthened and toughened by lamella structure" . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING 734 (2018) : 311-317 .
APA Sun, Junjie , Jiang, Tao , Wang, Yingjun , Guo, Shengwu , Liu, Yongning . Ultrafine grained dual-phase martensite/ferrite steel strengthened and toughened by lamella structure . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2018 , 734 , 311-317 .
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A low-alloy high-carbon martensite steel with 2.6 GPa tensile strength and good ductility EI SCIE Scopus
期刊论文 | 2018 , 158 , 247-256 | ACTA MATERIALIA
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A low-alloy and high-carbon martensite steel (0.66% C) with ultrafine grains is produced by combination of Tempforming (tempering and deforming of a quenched steel) and reheating followed by water quenching and low temperature tempering. The size of prior-austenite grains of the steel is reduced to 2.4 mu m through this new technique, and its ultimate tensile strength of 2.6 GPa and elongation of 7% are obtained, which is the highest strength in low alloy high strength steels. The microstructure of the high carbon martensite consists of high density dislocations, undissolved spherical carbides, and dispersed nano-scale Fe3C and Fe5C2\ phases precipitated at interior of martensitic after tempering. The strengthening mechanisms of the ultrafine grain martensitic steel are mainly dislocation strengthening and precipitation strengthening and also fine grain strengthening. The tensile strength and ductility of the steel are superior to that of existing maraging steels, such as C350, the highest strength in commercialized level, in which more than 20% precious alloy elements such as Co, Mo, Ni, and Ti are contained, and the cost of our materials is only about 1/50 of the C350. All above advantages are desirable for broad industrial applications at an economic cost. (C) 2018 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Keyword :

Dislocation substructure Ductility High carbon martensite steel Ultrafine grain Ultrahigh strength

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GB/T 7714 Wang, Yingjun , Sun, Junjie , Jiang, Tao et al. A low-alloy high-carbon martensite steel with 2.6 GPa tensile strength and good ductility [J]. | ACTA MATERIALIA , 2018 , 158 : 247-256 .
MLA Wang, Yingjun et al. "A low-alloy high-carbon martensite steel with 2.6 GPa tensile strength and good ductility" . | ACTA MATERIALIA 158 (2018) : 247-256 .
APA Wang, Yingjun , Sun, Junjie , Jiang, Tao , Sun, Yu , Guo, Shengwu , Liu, Yongning . A low-alloy high-carbon martensite steel with 2.6 GPa tensile strength and good ductility . | ACTA MATERIALIA , 2018 , 158 , 247-256 .
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Enhanced Structural Stability of Nickel-Cobalt Hydroxide via Intrinsic Pillar Effect of Metaborate for High-Power and Long-Life Supercapacitor Electrodes SCIE PubMed
期刊论文 | 2017 , 17 (1) , 429-436 | NANO LETTERS | IF: 12.08
WoS CC Cited Count: 59
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Abstract :

Layered alpha-Ni(OH)(2) and its, derivative bimetallic hydroxides (e.g., alpha-(Ni/Co)(OH)(2)) have attracted much attention due to their high Specific capacitance, although their insufficient cycling stability has blocked their wide application in various technologies. In this work; we demonstrate that the cycling performance of alpha-(Ni/Co)(OH)(2) can be obviously enhanced via the intrinsic pillar effect of metaborate. Combining the high porosity feature of the metaborate stabilized alpha-(Ni/CO)(OH)(2) and the improved electronic conductivity Offered by graphene substrate, the average capacitance fading rate of the metaborate stabilized alpha-(Ni/Co)(OH)(2) is only similar to 0.0017% per cycle within 10 000 cycles at the current density of 5 A g(-1). The rate performance is excellent over a wide temperature range from -20 to 40 degrees C. We believe that the enhancements should mainly be ascribed to the excellent structural stability offered by the metaborate pillars, and the detailed mechanism is discussed.

Keyword :

bimetallic hydroxides Pillar effect graphene metaborate supercapacitor

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GB/T 7714 Chen, Yuanzhen , Pang, Wei Kong , Bai, Haihua et al. Enhanced Structural Stability of Nickel-Cobalt Hydroxide via Intrinsic Pillar Effect of Metaborate for High-Power and Long-Life Supercapacitor Electrodes [J]. | NANO LETTERS , 2017 , 17 (1) : 429-436 .
MLA Chen, Yuanzhen et al. "Enhanced Structural Stability of Nickel-Cobalt Hydroxide via Intrinsic Pillar Effect of Metaborate for High-Power and Long-Life Supercapacitor Electrodes" . | NANO LETTERS 17 . 1 (2017) : 429-436 .
APA Chen, Yuanzhen , Pang, Wei Kong , Bai, Haihua , Zhou, Tengfei , Liu, Yongning , Li, Sai et al. Enhanced Structural Stability of Nickel-Cobalt Hydroxide via Intrinsic Pillar Effect of Metaborate for High-Power and Long-Life Supercapacitor Electrodes . | NANO LETTERS , 2017 , 17 (1) , 429-436 .
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Lithium-Rich Cathode Materials for High Energy-Density Lithium-Ion Batteries SCIE Scopus CSCD PKU
期刊论文 | 2017 , 29 (2-3) , 198-209 | PROGRESS IN CHEMISTRY | IF: 0.82
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Abstract :

With the development of mobile communication equipment and electric cars, there is an, increasing demand for high capacity lithium-ion batteries. It is difficult for the present commercialized lithium-ion power batteries to meet the requirement of one charge to travel above 500 km, because of low discharge capacity, like lithium iron phosphate and ternary cathode material, possessing the discharge capacity lower than 180 mAh/g. Therefore, the specific capacity of cathode materials has become a bottleneck to increase the energy density of lithium-ion batteries. Lithium-rich cathode materials with large specific capacity (>= 250 mAh/g), high discharge voltage (3. 8 V), and high theory energy density (900 Wh/kg) are thought as ideal cathode material of power batteries for electric cars in the future, so, it is of great realistic significance to study the lithium-rich cathode materials with high specific capacity. This paper reviews the development of cathode materials for lithium-ion batteries as well as the situation of recent commercial cathode materials with low specific capacity. Structures and electrochemical properties of lithium-rich cathode materials as a new next-generation higher capacity are summarized, and the discharge mechanism and the latest progress in modifications are presented. Moreover, some problems related with lithium-rich materials for high energy-density lithium-ion batteries are presented, followed by the corresponding ideas and approaches of solution.

Keyword :

surface coating lithium-rich materials layered-spinel transformation lithium-ion batteries

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GB/T 7714 Yan, Wuwei , Liu, Yongning , Chong, Shaokun et al. Lithium-Rich Cathode Materials for High Energy-Density Lithium-Ion Batteries [J]. | PROGRESS IN CHEMISTRY , 2017 , 29 (2-3) : 198-209 .
MLA Yan, Wuwei et al. "Lithium-Rich Cathode Materials for High Energy-Density Lithium-Ion Batteries" . | PROGRESS IN CHEMISTRY 29 . 2-3 (2017) : 198-209 .
APA Yan, Wuwei , Liu, Yongning , Chong, Shaokun , Zhou, Yaping , Liu, Jianguo , Zou, Zhigang . Lithium-Rich Cathode Materials for High Energy-Density Lithium-Ion Batteries . | PROGRESS IN CHEMISTRY , 2017 , 29 (2-3) , 198-209 .
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A lamellar structured ultrafine grain ferrite-martensite dual-phase steel and its resistance to hydrogen embrittlement EI SCIE Scopus
期刊论文 | 2017 , 698 , 390-399 | JOURNAL OF ALLOYS AND COMPOUNDS | IF: 3.779
WoS CC Cited Count: 6 SCOPUS Cited Count: 10
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Abstract :

A lamellar structured ultrafine grain dual-phase (UFG DP) steel was prepared by intercritical annealing and subsequent warm rolling of a low-carbon martensite steel. The ultrafine structure is composed of alternate ferrite and martensite strips (i.e., lamellar structure) parallel to the rolling direction, and the strips are composted of very fine grains in an average size of 0.96 mm. Hydrogen embrittlement (HE) of the UFG DP steel was investigated by a slow strain rate tensile (SSRT) of hydrogen charged specimens. Compared with uniform structured steel obtained in normal quenching and tempering (QT) technology, the UFG DP steel exhibits markedly high resistance to HE at a tensile strength level of 1300 MPa. A fracture model based on plastic zone and stress distribution was proposed to explain the fracture process. The lamellar structure leaves weaker ferrite/martensite interface parallel to the longitudinal direction that leads to delamination, which relaxes stress concentration and makes crack deflection, resulting in the higher HE resistance of the lamellar structured UFG DP steel. Moreover, the UFG structure increases fracture strength that also increases HE resistance. (C) 2016 Elsevier B.V. All rights reserved.

Keyword :

Hydrogen embrittlement Delamination fracture Ultrafine grain dual-phase steel Ferrite Martensite

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GB/T 7714 Sun, Junjie , Jiang, Tao , Sun, Yu et al. A lamellar structured ultrafine grain ferrite-martensite dual-phase steel and its resistance to hydrogen embrittlement [J]. | JOURNAL OF ALLOYS AND COMPOUNDS , 2017 , 698 : 390-399 .
MLA Sun, Junjie et al. "A lamellar structured ultrafine grain ferrite-martensite dual-phase steel and its resistance to hydrogen embrittlement" . | JOURNAL OF ALLOYS AND COMPOUNDS 698 (2017) : 390-399 .
APA Sun, Junjie , Jiang, Tao , Sun, Yu , Wang, Yingjun , Liu, Yongning . A lamellar structured ultrafine grain ferrite-martensite dual-phase steel and its resistance to hydrogen embrittlement . | JOURNAL OF ALLOYS AND COMPOUNDS , 2017 , 698 , 390-399 .
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A high performance martensitic stainless steel containing 1.5 wt% Si EI SCIE Scopus
期刊论文 | 2017 , 125 , 35-45 | MATERIALS & DESIGN | IF: 4.525
WoS CC Cited Count: 2 SCOPUS Cited Count: 3
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Abstract :

Usually, martensitic precipitation hardening stainless steels (MPHSSs) contain ultralow carbon concentration to ensure its high performance in corrosion resistance, weldability and toughness. Meanwhile, high content of alloy elements (such as Mo, Ni, Ti and Cu) is inevitably added in order to obtain superb strength by precipitation hardening. In this work, a new idea of alloying design in stainless steels has been proposed, in which carbon serves as the main strengthening element and high silicon concentration (1.5 wt%) is used to suppress carbide precipitation and coarsening during tempering. A steel with composition of Fe-0.2C-15Cr-3Ni-1.5Si-1.0Mn has been designed and prepared, and its excellent mechanical performance (ultimate tensile strength of 1680 MPa, total elongation of 16%), pitting corrosion resistance and weldability have been displayed. Moreover only low-cost alloying components and ordinary treatments are needed to obtain those outstanding properties which are comparable to commercialized MPHSSs (such as 17-4 PH, PH13-8 Mo). (C) 2017 Elsevier Ltd. All rights reserved.

Keyword :

Solution strengthening Stainless steel Mechanical property Alloying design

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GB/T 7714 Jiang, Tao , Sun, Junjie , Liu, Hongji et al. A high performance martensitic stainless steel containing 1.5 wt% Si [J]. | MATERIALS & DESIGN , 2017 , 125 : 35-45 .
MLA Jiang, Tao et al. "A high performance martensitic stainless steel containing 1.5 wt% Si" . | MATERIALS & DESIGN 125 (2017) : 35-45 .
APA Jiang, Tao , Sun, Junjie , Liu, Hongji , Wang, Yingjun , Guo, Shengwu , Sun, Yu et al. A high performance martensitic stainless steel containing 1.5 wt% Si . | MATERIALS & DESIGN , 2017 , 125 , 35-45 .
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Super-strong dislocation-structured high-carbon martensite steel SCIE PubMed Scopus
期刊论文 | 2017 , 7 | SCIENTIFIC REPORTS | IF: 4.122
WoS CC Cited Count: 2 SCOPUS Cited Count: 2
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High-carbon martensite steels (with C > 0.5 wt.%) are very hard but at the same time as brittle as glass in as-quenched or low-temperature-tempered state. Such extreme brittleness, originating from a twin microstructure, has rendered these steels almost useless in martensite state. Therefore, for more than a century it has been a common knowledge that high-carbon martensitic steels are intrinsically brittle and thus are not expected to find any application in harsh loading conditions. Here we report that these brittle steels can be transformed into super-strong ones exhibiting a combination of ultrahigh strength and significant toughness, through a simple grain-refinement treatment, which refines the grain size to similar to 4 mu m. As a result, an ultra-high tensile strength of 2.4 similar to 2.6 GPa, a significant elongation of 4 similar to 10% and a good fracture toughness (K-1C) of 23.5 similar to 29.6 MPa m(1/2) were obtained in high-carbon martensitic steels with 0.61-0.65 wt.% C. These properties are comparable with those of "the king of super-high-strength steels"-maraging steels, but achieved at merely 1/30 similar to 1/50 of the price. The drastic enhancement in mechanical properties is found to arise from a transition from the conventional twin microstructure to a dislocation one by grain refinement. Our finding may provide a new route to manufacturing super-strong steels in a simple and economic way.

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GB/T 7714 Sun, Jun-jie , Liu, Yong-ning , Zhu, Yun-tian et al. Super-strong dislocation-structured high-carbon martensite steel [J]. | SCIENTIFIC REPORTS , 2017 , 7 .
MLA Sun, Jun-jie et al. "Super-strong dislocation-structured high-carbon martensite steel" . | SCIENTIFIC REPORTS 7 (2017) .
APA Sun, Jun-jie , Liu, Yong-ning , Zhu, Yun-tian , Lian, Fu-liang , Liu, Hong-ji , Jiang, Tao et al. Super-strong dislocation-structured high-carbon martensite steel . | SCIENTIFIC REPORTS , 2017 , 7 .
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