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Quantitative reorientation behaviors of macro-twin interfaces in shape-memory alloy under compression stimulus in situ TEM EI
期刊论文 | 2022 , 107 , 243-251 | Journal of Materials Science and Technology
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Abstract :

Twinning stress is known to be a critical factor for the actuating performance of magnetic shape memory alloys because of the harmful deterioration of their magnetic field-induced strain effect. However, the intrinsic origin of the high twinning stress is still in debate. In this work, we firstly fill this gap by precisely probing the reorientation behaviors of A-C and A-B two common macro-twin interfaces under the stimulus of uniaxial compression in-situ transmission electron microscope. The grain boundary is proved to be the main reason for large twinning stress. The twinning stress of the A-C and A-B type interfaces quantitatively are ∼0.69 and 1.27 MPa within the plate respectively. The A-C type interface evidently has smaller twinning stress and larger deformation variable than the A-B interface. Under the action of compression, not only the orientations of the crystals have changed, but also the roles of the major and minor lamellae have changed for both interfaces due to the movements of twinning dislocations. Combining in-situ and quasi in-situ electron diffraction data, the reorientation process is clearly and intuitively shown by the stereographic projection. Atomic models and the theory of dislocation motion are proposed to phenomenologically clarify the intrinsic mechanism. This work is believed to not only provide a deeper understanding of the deformation mechanism of magnetic shape memory alloys under uniaxial compression testing, but also discover that compression training is not the mechanical training way to decrease the twinning stress of non-modulated martensite in single crystal shape memory alloys. © 2021

Keyword :

Magnetism Martensite Compression testing Single crystals Shape-memory alloy Deterioration Deformation Transmission electron microscopy Textures Twinning Grain boundaries

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GB/T 7714 Chen, Bin , Guan, Chaoshuai , Li, Yong et al. Quantitative reorientation behaviors of macro-twin interfaces in shape-memory alloy under compression stimulus in situ TEM [J]. | Journal of Materials Science and Technology , 2022 , 107 : 243-251 .
MLA Chen, Bin et al. "Quantitative reorientation behaviors of macro-twin interfaces in shape-memory alloy under compression stimulus in situ TEM" . | Journal of Materials Science and Technology 107 (2022) : 243-251 .
APA Chen, Bin , Guan, Chaoshuai , Li, Yong , Yang, Chong , Zhang, Junwei , Liu, Gang et al. Quantitative reorientation behaviors of macro-twin interfaces in shape-memory alloy under compression stimulus in situ TEM . | Journal of Materials Science and Technology , 2022 , 107 , 243-251 .
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Effect of Microalloying Addition on Microstructure and Mechanical Properties of Ni-W Coatings EI SCIE
期刊论文 | 2021 , 50 (1) , 145-152 | Rare Metal Materials and Engineering
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Abstract :

The effect of processing technology and microalloying addition on the microstructure and mechanical properties of Ni-W coatings prepared by electrodeposition was studied. The surface morphology, microstructure, and tensile properties of Ni-W coatings were studied with a small W addition of less than 2.0at%. The results show that the Ni-W coatings have a single-phase fcc structure. By increasing the W content, the surface morphology of the coatings varies from the grooves between the coarse pyramid structures to uniformly distributed micropores. At the same time, the intensity of Ni(220) diffraction peak of the coatings is also gradually weakened, with the reduction of surface roughness and the grain size. There is a critical W addition of about 1.0at%, where the yield strength of Ni-W coating increases sharply from ~1.0 GPa at the W addition 1.0at%. However, the tensile elongation is insensitive to the W content, which keep almost unchanged within the studied W addition range. In addition, strain hardening capacity of the coatings is also stable with the W content. In this work, the mechanical properties of Ni-W coating with micro-addition of W are optimized through manipulation of microalloying effect on the surface defect and microstructure. © 2021, Science Press. All right reserved.

Keyword :

Microstructure Surface roughness Binary alloys Microalloying Morphology Coatings Mechanical properties Strain hardening Surface defects Surface morphology

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GB/T 7714 Cheng, Lu , Wang, Yaqiang , Zhang, Jinyu et al. Effect of Microalloying Addition on Microstructure and Mechanical Properties of Ni-W Coatings [J]. | Rare Metal Materials and Engineering , 2021 , 50 (1) : 145-152 .
MLA Cheng, Lu et al. "Effect of Microalloying Addition on Microstructure and Mechanical Properties of Ni-W Coatings" . | Rare Metal Materials and Engineering 50 . 1 (2021) : 145-152 .
APA Cheng, Lu , Wang, Yaqiang , Zhang, Jinyu , Liu, Gang , Sun, Jun . Effect of Microalloying Addition on Microstructure and Mechanical Properties of Ni-W Coatings . | Rare Metal Materials and Engineering , 2021 , 50 (1) , 145-152 .
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Alloying effects on the microstructure and mechanical properties of nanocrystalline Ti-based alloyed thin films EI SCIE PubMed
期刊论文 | 2021 , 13 (39) , 16649-16661 | NANOSCALE
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Abstract :

Ti-based films alloyed with various Ta or Zr contents were deposited on a Si (100) substrate by magnetron sputtering. Transmission electron microscopy observations suggested that the solute Ta and Zr atoms distributed uniformly in the matrix Ti, refining the grain size. The microstructure transformed from single phase alpha-Ti to the coexistence of (alpha + beta)-Ti when the Ta addition was increased to 18.2 at%. Hardness and strain rate sensitivity of the Ti-based alloyed films were evaluated by nanoindentation experiments, to show the effects of constituents and their contents. The hardness was found to change non-monotonously within the studied Ta or Zr range, which could be explained by alloying dependence of the strengthening mechanisms, including partial dislocation mechanism emanating from grain boundaries, solid solution strengthening, and solution pinning strengthening. Furthermore, a mechanistic model based on partial dislocation inhomogeneous nucleation was employed to describe the composition-dependent strain rate sensitivity of the alloyed Ti films.

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GB/T 7714 Hou, Zhaoqi , Zhang, Jinyu , Zhang, Peng et al. Alloying effects on the microstructure and mechanical properties of nanocrystalline Ti-based alloyed thin films [J]. | NANOSCALE , 2021 , 13 (39) : 16649-16661 .
MLA Hou, Zhaoqi et al. "Alloying effects on the microstructure and mechanical properties of nanocrystalline Ti-based alloyed thin films" . | NANOSCALE 13 . 39 (2021) : 16649-16661 .
APA Hou, Zhaoqi , Zhang, Jinyu , Zhang, Peng , Wu, Kai , Wang, Yaqiang , Liu, Gang et al. Alloying effects on the microstructure and mechanical properties of nanocrystalline Ti-based alloyed thin films . | NANOSCALE , 2021 , 13 (39) , 16649-16661 .
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Superior strength-ductility synergy and strain hardenability of Al/Ta co-doped NiCoCr twinned medium entropy alloy for cryogenic applications EI SCIE
期刊论文 | 2021 , 220 | ACTA MATERIALIA
WoS CC Cited Count: 1
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Abstract :

Metallic materials with outstanding cryogenic mechanical properties are highly demanded for cryogenic engineering applications. Here we developed a novel (NiCoCr)(92)Al6Ta2 medium-entropy alloy (MEA) towards superior cryogenic mechanical properties via elaborating the chemical composition designing and the thermo-mechanical processing. It appears that the twinned (NiCoCr)(92)Al6Ta2 MEA shows a strongly temperature-dependent mechanical behavior, i.e., when the testing temperature from 298 down to 77 K, the yield strength, ultimate strength and tensile ductility are increased from similar to 600 to similar to 800 MPa, from similar to 1.0 to similar to 1.35 GPa and from similar to 52% to similar to 90%, respectively. An excellent strength-ductility synergy and extraordinary strain hardening capacity were realized in this alloy, in particular the product of tensile strength and elongation is more superior to their reported counterparts. There is a strongly temperature dependent deformation mechanism transition from the ordinary planar-slip at 298 K to the cooperative plastic mechanisms at 77 K, including stacking faults (SFs) and deformation twins. The excellent cryogenic mechanical properties of this designed MEA stems from the synergic effects of nanotwins, hierarchical SFs and Lomer-Cottrell locks, as well as their extensive interactions, rarely observed in their siblings deformed at room temperature. Furthermore, the deformation twinning acting as an additional/significant mechanism for plasticity and favoring strain hardening, along with the effect of temperature-dependent dislocation-twin interactions, collaboratively delays the onset of necking for enhanced ductility at 77 K. (C) 2021 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Keyword :

Cryogenic temperature Mechanical properties Strain hardening Medium-entropy alloy Deformation mechanisms

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GB/T 7714 Zhang, D. D. , Zhang, J. Y. , Kuang, J. et al. Superior strength-ductility synergy and strain hardenability of Al/Ta co-doped NiCoCr twinned medium entropy alloy for cryogenic applications [J]. | ACTA MATERIALIA , 2021 , 220 .
MLA Zhang, D. D. et al. "Superior strength-ductility synergy and strain hardenability of Al/Ta co-doped NiCoCr twinned medium entropy alloy for cryogenic applications" . | ACTA MATERIALIA 220 (2021) .
APA Zhang, D. D. , Zhang, J. Y. , Kuang, J. , Liu, G. , Sun, J. . Superior strength-ductility synergy and strain hardenability of Al/Ta co-doped NiCoCr twinned medium entropy alloy for cryogenic applications . | ACTA MATERIALIA , 2021 , 220 .
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Hierarchical structure in Al-Cu alloys to promote strength/ductility synergy EI SCIE
期刊论文 | 2021 , 202 | SCRIPTA MATERIALIA
WoS CC Cited Count: 2
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Abstract :

Experimental evidence demonstrated that equal channel angular pressing (ECAP) at cryogenic temperature, in comparison with ECAP at room temperature, led to promoted strength-ductility synergy in an Al-2.5wt.%Cu alloy. The simultaneous improvement is related to microstructural hierarchy of multimodal grains, low angle grain boundaries, and inter/intragranular precipitates, which was tuned by aging treatment in match with the low-temperature ECAP. The artificial aging could maintain multimodal grain size distribution, introduce a large number of low angle grain boundaries and produce intragranular precipitates to improve strength/ductility. A minor 0.3wt.% Sc addition was effective in optimizing the precipitations and further boosting the strength/ductility combination. The underlying mechanisms for higher strength and greater ductility were rationalized in terms of the low-temperature ECAP.& nbsp; (c) 2021 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Keyword :

Al-Cu alloy Mechanical properties Microalloying effect Ultrafine-grained Hierarchical microstructure

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GB/T 7714 Wu, S. H. , Xue, H. , Yang, C. et al. Hierarchical structure in Al-Cu alloys to promote strength/ductility synergy [J]. | SCRIPTA MATERIALIA , 2021 , 202 .
MLA Wu, S. H. et al. "Hierarchical structure in Al-Cu alloys to promote strength/ductility synergy" . | SCRIPTA MATERIALIA 202 (2021) .
APA Wu, S. H. , Xue, H. , Yang, C. , Kuang, J. , Zhang, P. , Zhang, J. Y. et al. Hierarchical structure in Al-Cu alloys to promote strength/ductility synergy . | SCRIPTA MATERIALIA , 2021 , 202 .
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Solute cluster evolution during deformation and high strain hardening capability in naturally aged Al-Zn-Mg alloy EI SCIE
期刊论文 | 2021 , 207 | ACTA MATERIALIA
WoS CC Cited Count: 4
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Abstract :

The natural aging (NA) response of a commercial Al-Zn-Mg alloy has been tracked to investigate the effects of solute clusters on its mechanical properties. It has been observed that the increase of yield strength during NA is not accompanied by the degradation of uniform elongation due to the simultaneously enhanced strain hardening ability. As a consequence, the Al-Zn-Mg alloy with dense solute clusters shows a comparable yield strength, better strain hardening ability and uniform tensile strain relative to its artificially aged counterparts containing precipitates. This positive effect of solute clusters on strain hardening has been systematically studied by tracing the microstructure evolution during deformation through synchrotron X-ray diffraction and atom probe tomography. We found that the dislocation multiplication dominates over the entire deformation process until failure in NA alloys; however, no effect of solute clusters on the dislocation density evolution can be identified. On the other hand, solute clusters themselves dramatically evolve, showing a dissolution-to-coarsening transition during deformation, which can be understood on the basis of a kinetic model. The experimental evidence strongly suggest that the dislocation storage and strain-induced evolution of solute clusters are insufficient to account for the observed high strain hardening rate, and the contribution from other possible mechanisms are estimated in a semi-quantitative manner. (C) 2021 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Keyword :

Solute clustering Strain hardening 7XXX aluminum alloys Strengthening

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GB/T 7714 Zhang, Peng , Shi, Kunkun , Bian, Jianjun et al. Solute cluster evolution during deformation and high strain hardening capability in naturally aged Al-Zn-Mg alloy [J]. | ACTA MATERIALIA , 2021 , 207 .
MLA Zhang, Peng et al. "Solute cluster evolution during deformation and high strain hardening capability in naturally aged Al-Zn-Mg alloy" . | ACTA MATERIALIA 207 (2021) .
APA Zhang, Peng , Shi, Kunkun , Bian, Jianjun , Zhang, Jinyu , Peng, Yong , Liu, Gang et al. Solute cluster evolution during deformation and high strain hardening capability in naturally aged Al-Zn-Mg alloy . | ACTA MATERIALIA , 2021 , 207 .
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Effect of Si addition on the precipitation and mechanical/electrical properties of dilute Al-Zr-Sc alloys EI SCIE
期刊论文 | 2021 , 812 | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
WoS CC Cited Count: 1
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Abstract :

Microstructural evolution and mechanical/electrical properties of aged Al-0.2 wt%Zr-0.05 wt%Sc alloys with different Si additions (0, 0.05, 0.10 and 0.15 wt%) were comparatively studied by using transmission electron microscopy, electrical conductivity measurements, and microhardness measurements. A significant Si addition effect was demonstrated that the Si addition accelerated the precipitation kinetics and enhanced the heterogeneous precipitation of Al-3(Sc, Zr) nanoparticles. However, both the peak-aging temperature and peak microhardness during isochronal aging were insensitive to the Si addition. The underlying mechanism is related to a partitioning effect of Si among Sc, Zr and vacancy that produces a saturated concentration of Si-vacancy clusters to serve as heterogeneous nuclei. It was further manifested that dual-scale particles, i.e., Al3Zr dispersoids and Al-3(Sc1-xZrx) nanoprecipitates in different length scales, could be produced by deliberately designing the heat treatment protocol. A coupling effect of the dual-scale particles led to an enhanced threshold stress in high-temperature creep testing, indicative of an improved creep resistance promoted by the minor Si addition. Moreover, the recrystallization resistance was seldom affected by Si addition, while slightly improved by introducing dual-scale particles.

Keyword :

Creep resistance Al alloys Recrystallization resistance Dual-scale particles

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GB/T 7714 Wu, S. H. , Xue, H. , Yang, C. et al. Effect of Si addition on the precipitation and mechanical/electrical properties of dilute Al-Zr-Sc alloys [J]. | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2021 , 812 .
MLA Wu, S. H. et al. "Effect of Si addition on the precipitation and mechanical/electrical properties of dilute Al-Zr-Sc alloys" . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING 812 (2021) .
APA Wu, S. H. , Xue, H. , Yang, C. , Cheng, P. M. , Zhang, P. , Kuang, J. et al. Effect of Si addition on the precipitation and mechanical/electrical properties of dilute Al-Zr-Sc alloys . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2021 , 812 .
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On the Texture Weakening During Electropulse Annealing Treatment of Mg-1Ce Alloy: The Role of Nucleation and Nucleus Growth SCIE Scopus
期刊论文 | 2020 , 51 (12) , 6640-6657 | METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE
SCOPUS Cited Count: 3
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Abstract :

Mg-1Ce alloys were pre-rolled at room temperature to various reductions to achieve different as-rolled microstructures. The deformed materials were then treated with a pulsed electric current (electropulse treatment, EPT) to study the effect of the as-rolled microstructure on the recrystallization texture formation. The experimental results show that an optimum window exists for pre-rolling reductions, within which the as-rolled microstructures and sharp basal textures obtained will evolve into fine recrystallized grains and weak textures during the subsequent EPT. Microstructure analysis indicates a competition between two processes, the nucleation and the nucleus growth, in contributing to the texture weakening of the alloy. While both the application of pulsed electric current and the increase in the pre-rolling reductions could strengthen the advantage of the nucleation rate of the non-basal nuclei over those with basal orientations, the contribution from nucleus growth depends mainly on the available deformed basal-oriented matrix, which decreases with increasing pre-rolling reductions. The results of the present study might provide useful guidance for the optimization of process parameters in the future application of the 'pre-rolling + EPT' technique on the Mg alloy sheet.

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GB/T 7714 Kuang, Jie , Du, Xinpeng , Al-Samman, Talal et al. On the Texture Weakening During Electropulse Annealing Treatment of Mg-1Ce Alloy: The Role of Nucleation and Nucleus Growth [J]. | METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE , 2020 , 51 (12) : 6640-6657 .
MLA Kuang, Jie et al. "On the Texture Weakening During Electropulse Annealing Treatment of Mg-1Ce Alloy: The Role of Nucleation and Nucleus Growth" . | METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE 51 . 12 (2020) : 6640-6657 .
APA Kuang, Jie , Du, Xinpeng , Al-Samman, Talal , Li, Xiaohui , Liu, Gang , Sun, Jun . On the Texture Weakening During Electropulse Annealing Treatment of Mg-1Ce Alloy: The Role of Nucleation and Nucleus Growth . | METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE , 2020 , 51 (12) , 6640-6657 .
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Cluster-growth kinetics, plastic deformation and fracture in naturally aged Al-Zn-Mg alloy EI CSCD
期刊论文 | 2020 , 30 (11) , 2513-2525 | Chinese Journal of Nonferrous Metals
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Abstract :

The clusters growth kinetics and the deformation properties in natural-aged Al-Zn-Mg alloy were investigated by electrical conductivity, microhardness and tensile tests. Multiple characterization methods including SEM, TEM, APT and XRD were applied to reveal the microstructure features. The results show that through the natural aging of about 1000 h, the high number density of solute clusters forms in 7B05 alloy and are responsible for the natural aging hardening effect. Natural-aged Al-Zn-Mg alloy exhibits better strain-hardening properties and uniform elongation than their thermally treated counterparts. The presence of shearing-resistant precipitates in thermal-treated alloys results in rapid accumulation of dislocation loops around precipitates at small strain whereas at large strain, the dislocation dynamic recovery process is dominant. In natural-aged Al-Zn-Mg alloy, the dislocation recovery is inhibited by solutes and clusters, meanwhile, the dynamic strain aging effect raises the resistance of dislocation movements, both leading to a greater strain-hardening capability. © 2020, Science Press. All right reserved.

Keyword :

Zinc alloys Metal testing Tensile testing Magnesium alloys Aluminum alloys Magnesium metallography Aluminum metallography Ternary alloys Strain hardening Growth kinetics Zinc metallography

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GB/T 7714 Shi, Kun-Kun , Zhao, Xiao-Long , Zhang, Peng et al. Cluster-growth kinetics, plastic deformation and fracture in naturally aged Al-Zn-Mg alloy [J]. | Chinese Journal of Nonferrous Metals , 2020 , 30 (11) : 2513-2525 .
MLA Shi, Kun-Kun et al. "Cluster-growth kinetics, plastic deformation and fracture in naturally aged Al-Zn-Mg alloy" . | Chinese Journal of Nonferrous Metals 30 . 11 (2020) : 2513-2525 .
APA Shi, Kun-Kun , Zhao, Xiao-Long , Zhang, Peng , Kuang, Jie , Zhang, Jin-Yu , Liu, Gang et al. Cluster-growth kinetics, plastic deformation and fracture in naturally aged Al-Zn-Mg alloy . | Chinese Journal of Nonferrous Metals , 2020 , 30 (11) , 2513-2525 .
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Heterogeneous microstructure-mediated ductile fracture of twin-roll cast Al-Mn strip EI SCIE Scopus
期刊论文 | 2020 , 783 | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | IF: 5.234
WoS CC Cited Count: 4 SCOPUS Cited Count: 5
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Abstract :

The microstructure and mechanical properties of the twin-roll cast (TRC) and traditional direct-chill cast (DC) Al-Mn strip have been compared using electron backscattered diffraction, scanning electron microscope, transmission electron microscope, and atom-probe tomography. The TRC Al-Mn strip showed a heterogeneous microstructure and texture along the thickness direction of the strip, forming a 'hard shell-soft core' structure. This heterogeneous microstructure resulted in a mutual constraint between the surface region and the center region, enabling the TRC strip to be plastically deformed to a total elongation >30% prior to fracture. In comparison, the DC strip, with a relatively homogeneous microstructure and texture, exhibited a uniform elongation close to zero. The distinct tensile properties presented by the two strips have been rationalized in terms of the differences in their microstructural features, including grain size/orientation, dislocation density, coarse constituent particles and solute atoms. A micromechanics model has been employed to understand the superior ductility of the TRC strip.

Keyword :

Twin-roll casting Al-Mn strip Heterogeneous structure Ductile fracture

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GB/T 7714 Zhao, X. L. , Kuang, J. , Shi, K. K. et al. Heterogeneous microstructure-mediated ductile fracture of twin-roll cast Al-Mn strip [J]. | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2020 , 783 .
MLA Zhao, X. L. et al. "Heterogeneous microstructure-mediated ductile fracture of twin-roll cast Al-Mn strip" . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING 783 (2020) .
APA Zhao, X. L. , Kuang, J. , Shi, K. K. , Zhang, P. , Xue, H. , Zhang, J. Y. et al. Heterogeneous microstructure-mediated ductile fracture of twin-roll cast Al-Mn strip . | MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING , 2020 , 783 .
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