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Rapidly Measuring Charge Carrier Mobility of Organic Semiconductor Films Upon a Point-contact Four-Probes Method Scopus SCIE
期刊论文 | 2019 , 7 (1) , 303-308 | IEEE Journal of the Electron Devices Society
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Abstract :

OAPA Field-effect mobility (&#x03BC;FET) of organic semiconductor films plays a key role in the performance of field-effect transistors (FETs). Numerical extraction of &#x03BC;FET from organic FET characteristics is not only time-consuming due to patterning of source/drain electrodes, but also frequently unreliable because of the contact resistances (Rc) between source/drain electrodes and semiconductors. Here we propose an approach to rapidly evaluate &#x03BC; by a point-contact four-probes method (&#x03BC;PFP) for organic semiconductor films. Four tip-like probes quickly contact the semiconductor film surface directly, without deposition of the conventional source/drain electrodes, to simultaneously inject current and measure the electric potential. The charge density and thus conductance of the film is manipulated upon scanning gate voltage, from which the extraction of &#x03BC;PFP, in good agreement with &#x03BC;FET, could be realized in a few seconds. This method, with easily-accessible setup and numerical model, substantially accelerates the evaluation of &#x03BC;PFP, and thus could help screen materials and optimize film morphology for organic FETs applications.

Keyword :

charge carrier mobility Electric potential Electrodes Films Logic gates Organic semiconductor films Organic semiconductors point-contact four-probes method. Probes Semiconductor device measurement

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GB/T 7714 Li, Dongfan , Li, Shengtao , Lu, Wanlong et al. Rapidly Measuring Charge Carrier Mobility of Organic Semiconductor Films Upon a Point-contact Four-Probes Method [J]. | IEEE Journal of the Electron Devices Society , 2019 , 7 (1) : 303-308 .
MLA Li, Dongfan et al. "Rapidly Measuring Charge Carrier Mobility of Organic Semiconductor Films Upon a Point-contact Four-Probes Method" . | IEEE Journal of the Electron Devices Society 7 . 1 (2019) : 303-308 .
APA Li, Dongfan , Li, Shengtao , Lu, Wanlong , Feng, Shi , Wei, Peng , Hu, Yupeng et al. Rapidly Measuring Charge Carrier Mobility of Organic Semiconductor Films Upon a Point-contact Four-Probes Method . | IEEE Journal of the Electron Devices Society , 2019 , 7 (1) , 303-308 .
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Dark Current Reduction Strategy via a Layer-By-Layer Solution Process for a High-Performance All-Polymer Photodetector. PubMed SCIE
期刊论文 | 2019 , 11 (8) , 8350-8356 | ACS applied materials & interfaces
WoS CC Cited Count: 3
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Abstract :

The ideal bulk-heterojunction for high-performance organic photodetectors prefers a morphology with a vertically gradient component to suppress the leaking current. Here, we demonstrate an all-polymer photodetector with a segregated bulk-heterojunction active layer. This all-polymer photodetector exhibits a dramatically reduced dark current density because of its built-in charge blocking layer, with a responsivity of 0.25 A W<sup>-1</sup> at a wavelength of approximately 600 nm and specific detectivity of 5.68 × 10<sup>12</sup> cm Hz<sup>1/2</sup> W<sup>-1</sup> as calculated from the noise spectra at 1 kHz. To our knowledge, this is among the best performances reported for photodetectors based on both polymeric donor and acceptor in the photoactive layer. These findings present a facile approach to improving the specific detectivity of polymer photodetectors via a layer-by-layer solution process.

Keyword :

noise spectral density gradient bulk heterojunction layer-by-layer process imide functionalized benzotriazole all-polymer photodetector

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GB/T 7714 Zhong Zhiming , Bu Laju , Zhu Peng et al. Dark Current Reduction Strategy via a Layer-By-Layer Solution Process for a High-Performance All-Polymer Photodetector. [J]. | ACS applied materials & interfaces , 2019 , 11 (8) : 8350-8356 .
MLA Zhong Zhiming et al. "Dark Current Reduction Strategy via a Layer-By-Layer Solution Process for a High-Performance All-Polymer Photodetector." . | ACS applied materials & interfaces 11 . 8 (2019) : 8350-8356 .
APA Zhong Zhiming , Bu Laju , Zhu Peng , Xiao Tong , Fan Baobing , Ying Lei et al. Dark Current Reduction Strategy via a Layer-By-Layer Solution Process for a High-Performance All-Polymer Photodetector. . | ACS applied materials & interfaces , 2019 , 11 (8) , 8350-8356 .
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Achieving High Doping Concentration by Dopant Vapor Deposition in Organic Solar Cells. PubMed SCIE
期刊论文 | 2019 , 11 (4) , 4178-4184 | ACS applied materials & interfaces
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Abstract :

Compared with the interfacial doping, molecular doping in bulk heterojunction (BHJ) is a more direct but challenging approach to optimize the photovoltaic performance in organic solar cells (OSCs). One of the main obstacles for its success is the low doping concentration because of the morphological damage. Starting from the phase diagram analysis, we discover that the unpreferred good miscibility between the p-type dopant and the acceptor leads to incorrect dopant dispersion, which reduces the achievable doping content. To overcome this, we use sequential doping by vapor annealing instead of blend solution doping, and we achieve the high doping concentration without sacrificing the blend film morphology. Benefiting from the undamaged film, we fulfill improved photovoltaic performance. Our positive results reveal the feasibility of high-level doping in complex organic BHJ films. It is believed that doping at high concentration potentially enlarges the extent of tunable range on electronic properties in OSCs and indicates greater improvement for device performance.

Keyword :

vapor doping organic solar cell Lewis acid doping sequential doping doped morphology high doping concentration

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GB/T 7714 Yan Han , Tang Yabing , Meng Xiangyi et al. Achieving High Doping Concentration by Dopant Vapor Deposition in Organic Solar Cells. [J]. | ACS applied materials & interfaces , 2019 , 11 (4) : 4178-4184 .
MLA Yan Han et al. "Achieving High Doping Concentration by Dopant Vapor Deposition in Organic Solar Cells." . | ACS applied materials & interfaces 11 . 4 (2019) : 4178-4184 .
APA Yan Han , Tang Yabing , Meng Xiangyi , Xiao Tong , Lu Guanghao , Ma Wei . Achieving High Doping Concentration by Dopant Vapor Deposition in Organic Solar Cells. . | ACS applied materials & interfaces , 2019 , 11 (4) , 4178-4184 .
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Manipulating Doping of Organic Semiconductors by Reactive Oxygen for Field-Effect Transistors EI SCIE Scopus
期刊论文 | 2018 , 12 (10) | PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS
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Thin film organic field-effect transistors (OFETs) are usually featured with charge traps, limiting charge transport and leading to low mobility especially at low gate voltages. In this work, doping process of a model organic semiconductor 2,7-didodecyl[1]benzothieno[3,2-b][1]benzothiophene (C12-BTBT) has been manipulated, using low-cost reactive oxygen namely oxygen plasma or ozone. It is found that low-pressure (20Pa) oxygen plasma can induce a low-moderate doping concentration, which is, however, sufficient to warrant field-effect mobilities over 5cm(2)V(-1)s(-1) in a large gate voltage range and sharp subthreshold swings, without degradation of on/off ratio. Low-pressure oxygen plasma can also positively shift the threshold voltage of the device, thus largely reducing the working voltages. Oxygen plasma with higher pressure than 100Pa induces higher doping concentration, more significantly shifting the threshold voltage and deteriorating on/off ratio due to substantial bulk electrical conductivity, which is similar to the treatment by UV-ozone at atmospheric pressure. As compared with the well-studied organic dopant F4-TCNQ, the doping process of reactive oxygen can be more easily in situ manipulated to reach an appropriate range of doping concentration, warranting higher performance and larger tunability for OFETs.

Keyword :

organic semiconductors doping charge transport oxygen plasma organic field-effect transistors

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GB/T 7714 Qiu, Yuming , Wei, Peng , Wang, Zihao et al. Manipulating Doping of Organic Semiconductors by Reactive Oxygen for Field-Effect Transistors [J]. | PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS , 2018 , 12 (10) .
MLA Qiu, Yuming et al. "Manipulating Doping of Organic Semiconductors by Reactive Oxygen for Field-Effect Transistors" . | PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS 12 . 10 (2018) .
APA Qiu, Yuming , Wei, Peng , Wang, Zihao , Lu, Wanlong , Jiang, Yihang , Zhang, Chaofan et al. Manipulating Doping of Organic Semiconductors by Reactive Oxygen for Field-Effect Transistors . | PHYSICA STATUS SOLIDI-RAPID RESEARCH LETTERS , 2018 , 12 (10) .
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Giant Transconductance of Organic Field-Effect Transistors in Compensation Electric Fields Scopus SCIE
期刊论文 | 2018 , 10 (5) | Physical Review Applied
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Abstract :

© 2018 American Physical Society. In field-effect transistors (FETs) that typically have three electrodes, the charge density and electrical conductance of semiconductor films are tuned by an electric field provided by the gate electrode. However, the other two electrodes (source and drain) are inevitably applied with different voltages to generate a source-drain current to make the FET work, which causes a continuous evolution of charge accumulation (or depletion) in the three-dimensional semiconducting films during gate-voltage scanning and thus leads to an intrinsic delay between on and off states. To avoid the delay and accelerate the switching speed, here we propose that transconductance of semiconducting films can be significantly increased (denoted as "giant transconductance" here) when the transport channel is within extra static compensation electric fields and experimentally verify it in organic FETs. The giant transconductance is theoretically derived as super transconductance, corresponding to an abrupt current variation at a fixed gate voltage and thus ideally zero subthreshold swing as well as infinite effective field-effect mobility (μFET). Giant transconductance is compatible with high temperature (up to 400 K), but both the doping concentration and the film thickness should be synergically optimized to warrant the super-rapid switching. For practical applications, we choose poly(3-hexylthiophene) and 2,7-didodecyl[1]benzothieno[3,2-b][1]benzothiophene to experimentally demonstrate the giant transconductance and its capability of current modulation. Giant transconductance could be potentially used in oscillator circuits, sensors, and high-performance circuits.

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GB/T 7714 Hu, Yupeng , Wei, Peng , Wang, Xudong et al. Giant Transconductance of Organic Field-Effect Transistors in Compensation Electric Fields [J]. | Physical Review Applied , 2018 , 10 (5) .
MLA Hu, Yupeng et al. "Giant Transconductance of Organic Field-Effect Transistors in Compensation Electric Fields" . | Physical Review Applied 10 . 5 (2018) .
APA Hu, Yupeng , Wei, Peng , Wang, Xudong , Bu, Laju , Lu, Guanghao . Giant Transconductance of Organic Field-Effect Transistors in Compensation Electric Fields . | Physical Review Applied , 2018 , 10 (5) .
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Organic-semiconductor: Polymer-electret blends for high-performance transistors EI Scopus SCIE
期刊论文 | 2018 , 11 (11) , 5835-5848 | Nano Research
WoS CC Cited Count: 2 SCOPUS Cited Count: 3
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Abstract :

As compared with polymer semiconductors, solution-processed small-molecule semiconductors usually have poorer film-formation properties, which induces wide variations in device performance in terms of mobility and threshold voltage, thus severely limiting their commercial applications. In this work, we propose an easily accessible method to improve the performance and reduce the variability of small-molecule organic field-effect transistors (OFETs) by blending organic semiconductors with an insulator polymer, which is subsequently post-treated by gate stress to generate an electret. By blending the organic semiconductor 2,7-didodecyl[1]benzothieno[3,2-b][1]benzothiophene (C12-BTBT) with the insulator polystyrene, uniform transport layers with vertically phase segregated morphology are obtained, from which the mobility and threshold voltage of OFETs are largely manipulated. The OFETs exhibit field-effect mobilities as high as 7.5 cm2·V−1·s−1with an on/off ratio exceeding 106in ambient conditions. This double-layer structure provides an appropriate architecture for applying gate-stress to inject charges into the insulating layer, forming an electret. The generation of the electret is thermally accelerated and thus can be easily realized under moderate gate-stress at elevated temperature (e.g., 60 °C). After cooling, the electret layer serves as a floating-gate, which not only continuously tunes the threshold voltage and field-effect mobility, but also helps minimize the contact resistances and optimize the subthreshold swing. As an application of this method, a digital inverter is built and its performance is optimized via in situ tuning of its individual transistors. [Figure not available: see fulltext.] © 2018 Tsinghua University Press and Springer-Verlag GmbH Germany, part of Springer Nature

Keyword :

Blending organic semiconductors C12-BTBT Commercial applications Double layer structure Field-effect mobilities Gate stress Organic electronics Vertical phase separations

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GB/T 7714 Wei, Peng , Li, Shengtao , Li, Dongfan et al. Organic-semiconductor: Polymer-electret blends for high-performance transistors [J]. | Nano Research , 2018 , 11 (11) : 5835-5848 .
MLA Wei, Peng et al. "Organic-semiconductor: Polymer-electret blends for high-performance transistors" . | Nano Research 11 . 11 (2018) : 5835-5848 .
APA Wei, Peng , Li, Shengtao , Li, Dongfan , Yu, Han , Wang, Xudong , Xu, Congcong et al. Organic-semiconductor: Polymer-electret blends for high-performance transistors . | Nano Research , 2018 , 11 (11) , 5835-5848 .
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Dual-Accepting-Unit Design of Donor Material for All-Small-Molecule Organic Solar Cells with Efficiency Approaching 11% EI SCIE
期刊论文 | 2018 , 30 (23) , 8661-8668 | Chemistry of Materials
WoS CC Cited Count: 7
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Abstract :

Design of high-performance small molecule donors for all-small-molecule organic solar cells (ASM-OSCs) requires a combinative effort of optimizing the material design and device fabrication. Herein, a new dual-accepting-unit medium-bandgap small molecule donor named SBDT-BDD is developed, which consists of a benzodithiophene (BDT) as the central electron-donating unit in combination with two rhodanines (A1) and two benzo-[1,2-c:4,5-c′]dithiophene-4,8-diones (BDD) (A2) as the electron-accepting units, forming a unique A1-A2-D-A2-A1 structure. The dual accepting units endow the SBDT-BDD with complementary absorption and appropriate energy level with fused-ring electron acceptor IDIC. Further investigations suggest that SBDT-BDD is morphologically compatible with the two acceptors of PC71BM and IDIC, benefiting the formation of ideal film morphology and efficient exciton dissociation as well as suppressed charge recombination in devices, resulting in outstanding current density and fill factor. The film-depth-dependent optical and electronic properties in such small molecule devices are synergistically optimized, to simultaneously manipulate photon harvesting contours and charge transport. The ASM-OSCs based on SBDT-BDD:IDIC blend produces a power conversion efficiency (PCE) of 9.2%, while the SBDT-BDD:IDIC:PC71BM ternary devices exhibit a significantly increased PCE of 10.9%. Upon molecule design to optimize morphology for precise manipulation of film-depth- and wavelength-dependent optical and electronic properties, this work provides a new strategy for a small molecule donor toward high-performance ASM-OSCs. © 2018 American Chemical Society.

Keyword :

Charge recombinations Device fabrications Electron-accepting units Exciton dissociation Optical and electronic properties Power conversion efficiencies Precise manipulation Small-molecule organic solar cells

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GB/T 7714 Huo, Yong , Gong, Xiao-Ting , Lau, Tsz-Ki et al. Dual-Accepting-Unit Design of Donor Material for All-Small-Molecule Organic Solar Cells with Efficiency Approaching 11% [J]. | Chemistry of Materials , 2018 , 30 (23) : 8661-8668 .
MLA Huo, Yong et al. "Dual-Accepting-Unit Design of Donor Material for All-Small-Molecule Organic Solar Cells with Efficiency Approaching 11%" . | Chemistry of Materials 30 . 23 (2018) : 8661-8668 .
APA Huo, Yong , Gong, Xiao-Ting , Lau, Tsz-Ki , Xiao, Tong , Yan, Cenqi , Lu, Xinhui et al. Dual-Accepting-Unit Design of Donor Material for All-Small-Molecule Organic Solar Cells with Efficiency Approaching 11% . | Chemistry of Materials , 2018 , 30 (23) , 8661-8668 .
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Reconstructing Space- and Energy-Dependent Exciton Generation in Solution-Processed Inverted Organic Solar Cells EI SCIE PubMed Scopus
期刊论文 | 2018 , 10 (16) , 13741-13747 | ACS APPLIED MATERIALS & INTERFACES
WoS CC Cited Count: 1 SCOPUS Cited Count: 1
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Photon absorption-induced exciton generation plays an important role in determining the photovoltaic properties of donor/acceptor organic solar cells with an inverted architecture. However, the reconstruction of light harvesting and thus exciton generation at different locations within organic inverted device are still not well resolved. Here, we investigate the film depth-dependent light absorption spectra in a small molecule donor/acceptor film. Including depth-dependent spectra into an optical transfer matrix method allows us to reconstruct both film depth- and energy-dependent exciton generation profiles, using which short-circuit current and external quantum efficiency of the inverted device are simulated and compared with the experimental measurements. The film depth-dependent spectroscopy, from which we are able to simultaneously reconstruct light harvesting profile, depth-dependent composition distribution, and vertical energy level variations, provides insights into photovoltaic process. In combination with appropriate material processing methods and device architecture, the method proposed in this work will help optimizing film depth-dependent optical/electronic properties for high-performance solar cells.

Keyword :

optical simulation inverted devices organic photovoltaics light absorption small molecule solar cells vertical phase separation

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GB/T 7714 Wang, Yuheng , Zhang, Yajie , Lu, Guanghao et al. Reconstructing Space- and Energy-Dependent Exciton Generation in Solution-Processed Inverted Organic Solar Cells [J]. | ACS APPLIED MATERIALS & INTERFACES , 2018 , 10 (16) : 13741-13747 .
MLA Wang, Yuheng et al. "Reconstructing Space- and Energy-Dependent Exciton Generation in Solution-Processed Inverted Organic Solar Cells" . | ACS APPLIED MATERIALS & INTERFACES 10 . 16 (2018) : 13741-13747 .
APA Wang, Yuheng , Zhang, Yajie , Lu, Guanghao , Feng, Xiaoshan , Xiao, Tong , Xie, Jing et al. Reconstructing Space- and Energy-Dependent Exciton Generation in Solution-Processed Inverted Organic Solar Cells . | ACS APPLIED MATERIALS & INTERFACES , 2018 , 10 (16) , 13741-13747 .
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Field-Effect Charge Transport in Doped Polymer Semiconductor-Insulator Alternating Bulk Junctions with Ultrathin Transport Layers. EI PubMed Scopus SCIE
期刊论文 | 2018 , 10 (45) , 39091-39099 | ACS applied materials & interfaces
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Conjugated-polymer field-effect transistors are attractive for flexible electronics. However, relatively high chemical doping (oxidation) concentration of p-type polymer semiconductors is usually not compatible with good transistor performance, due to poor switching-off capability and short-channel performance. Here, we propose a combined simulation and experimental investigation on charge transport in a semiconductor-insulator alternating bulk junction composed of repeating semiconductor and insulator regions, which shows better transistor performance at higher doping levels, as compared with traditional planar transistors. Moreover, the doped semiconductor transport layers in the junction should be less than 2 nm thick to ensure sufficient pinch-off capability. Using some semiconductors including poly(3-hexylthiophene), we utilize a fast solvent evaporation approach to obtain semiconductor-insulator alternating bulk junctions with ultrathin (thickness < 2 nm) semiconductor crystallites and with vertical gradients of both morphology and electronic properties. Doping with a concentration of up to 10<sup>19</sup> cm<sup>-3</sup> simultaneously induces the improvement of field-effect mobility, on/off ratio, and subthreshold swing, which leads to long-term (>1 year) stability, without lowering the short-channel performance. Moreover, these heterojunctions are optically transparent, nearly colorless, and flexible, thus could be exploited for wide electronic and photonic applications.

Keyword :

conjugated-polymers charge transport ultrathin layers field-effect transistors doping

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GB/T 7714 Hu Yupeng , Bu Laju , Wang Xudong et al. Field-Effect Charge Transport in Doped Polymer Semiconductor-Insulator Alternating Bulk Junctions with Ultrathin Transport Layers. [J]. | ACS applied materials & interfaces , 2018 , 10 (45) : 39091-39099 .
MLA Hu Yupeng et al. "Field-Effect Charge Transport in Doped Polymer Semiconductor-Insulator Alternating Bulk Junctions with Ultrathin Transport Layers." . | ACS applied materials & interfaces 10 . 45 (2018) : 39091-39099 .
APA Hu Yupeng , Bu Laju , Wang Xudong , Zhou Ling , Lu Guanghao . Field-Effect Charge Transport in Doped Polymer Semiconductor-Insulator Alternating Bulk Junctions with Ultrathin Transport Layers. . | ACS applied materials & interfaces , 2018 , 10 (45) , 39091-39099 .
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Critical Role of Vertical Phase Separation in Small-Molecule Organic Solar Cells EI SCIE Scopus
期刊论文 | 2018 , 10 (15) , 12913-12920 | ACS APPLIED MATERIALS & INTERFACES
WoS CC Cited Count: 2 SCOPUS Cited Count: 3
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Abstract :

An inverted device structure is a more stable configuration than a regular device structure for solution-processed organic solar cells (OSCs). However, most of the solution-processed small-molecule OSCs (SM-OSCs) reported in the literature used the regular device structure, and a regular device normally exhibits a higher efficiency than an inverted device. Herein, a representative small-molecule DR3TBDTT was selected to figure out the reason for photovoltaic performance differences between regular and inverted devices. The mechanisms for a reduced open-circuit voltage (V-oc) and fill factor (FF) in the inverted device were studied. The reduced V-oc and FF is due to the vertical phase separation with excess [6,6]-phenyl-C-71-butyric acid methyl ester near the air/blend surface, which leads to a reduction in build-in voltage and unbalanced charge transport in the inverted device. Another reason for the reduced FF is the unfavorable DR3TBDTT crystallite orientation distribution along the film thickness, which is preferential edge-on crystallites in the top layer of the blend film and the increased population of face-on crystallites in the bottom layer of the blend film. This study illustrates that the morphology plays a key role in photovoltaic performance difference between regular and inverted devices and provides useful guidelines for further optimization of the morphology of solution-processed SM-OSCs.

Keyword :

charge transport crystallite orientation open-circuit voltage loss small-molecule organic solar cells vertical phase separation

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GB/T 7714 Fang, Jin , Deng, Dan , Wang, Zaiyu et al. Critical Role of Vertical Phase Separation in Small-Molecule Organic Solar Cells [J]. | ACS APPLIED MATERIALS & INTERFACES , 2018 , 10 (15) : 12913-12920 .
MLA Fang, Jin et al. "Critical Role of Vertical Phase Separation in Small-Molecule Organic Solar Cells" . | ACS APPLIED MATERIALS & INTERFACES 10 . 15 (2018) : 12913-12920 .
APA Fang, Jin , Deng, Dan , Wang, Zaiyu , Adil, Muhammad Abdullah , Xiao, Tong , Wang, Yuheng et al. Critical Role of Vertical Phase Separation in Small-Molecule Organic Solar Cells . | ACS APPLIED MATERIALS & INTERFACES , 2018 , 10 (15) , 12913-12920 .
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