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Author:

Shu, Hua (Shu, Hua.) | Chen, Guoning (Chen, Guoning.) | Wang, Lu (Wang, Lu.) | Cui, Xia (Cui, Xia.) | Wang, Qun (Wang, Qun.) | Li, Wen (Li, Wen.) | Chang, Chun (Chang, Chun.) | Guo, Qi (Guo, Qi.) | Luo, Zhimin (Luo, Zhimin.) | Fu, Qiang (Fu, Qiang.)

Indexed by:

EI SCIE PubMed Engineering Village

Abstract:

A method is described for the functionalization of magnetic carbon nanotubes to recognize aristolochic acid and . 3-Glycidyloxypropyltrimethoxysilane was used as a coupling agent to immobilize adenine on a solid support. The morphology and structure of adenine-coated magnetic carbon nanotubes was investigated using transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and a vibrating sample magnetometer (VSM). The adsorption performance of the adenine-coated magnetic carbon nanotubes was evaluated via adsorption isotherms, the kinetics and selectivity tests. The adsorption capacity of the adenine-functionalized sorbent for aristolochic acid was determined to be 24.5 μg mg−1. By combining magnetic solid phase extraction with HPLC detection, a method was developed to enrich and detect aristolochic acids used in traditional Chinese medicine. A satisfactory recovery (92.7 - 97.5% for aristolochic acid and 92.6 - 99.4% for aristolochic acid ) and an acceptable relative standard deviation ( © 2020

Keyword:

Adsorption Coupling agents Extraction High resolution transmission electron microscopy Magnetism Medicine Multiwalled carbon nanotubes (MWCN) Nanotubes Phase separation Scanning electron microscopy

Author Community:

  • [ 1 ] [Shu, Hua]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 2 ] [Chen, Guoning]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 3 ] [Wang, Lu]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 4 ] [Cui, Xia]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 5 ] [Wang, Qun]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 6 ] [Li, Wen]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 7 ] [Chang, Chun]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 8 ] [Guo, Qi]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 9 ] [Luo, Zhimin]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China
  • [ 10 ] [Fu, Qiang]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China

Reprint Author's Address:

  • [Luo, Zhimin]School of Pharmacy, Xi'an Jiaotong University, Xi'an; 710061, China;;

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Source :

Journal of Chromatography A

ISSN: 0021-9673

Year: 2020

Volume: 1627

4 . 7 5 9

JCR@2020

4 . 7 5 9

JCR@2020

ESI Discipline: CHEMISTRY;

ESI HC Threshold:70

CAS Journal Grade:2

Cited Count:

WoS CC Cited Count: 9

SCOPUS Cited Count: 16

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 14

Affiliated Colleges:

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