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Abstract:
A method is described for the functionalization of magnetic carbon nanotubes to recognize aristolochic acid and . 3-Glycidyloxypropyltrimethoxysilane was used as a coupling agent to immobilize adenine on a solid support. The morphology and structure of adenine-coated magnetic carbon nanotubes was investigated using transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and a vibrating sample magnetometer (VSM). The adsorption performance of the adenine-coated magnetic carbon nanotubes was evaluated via adsorption isotherms, the kinetics and selectivity tests. The adsorption capacity of the adenine-functionalized sorbent for aristolochic acid was determined to be 24.5 μg mg−1. By combining magnetic solid phase extraction with HPLC detection, a method was developed to enrich and detect aristolochic acids used in traditional Chinese medicine. A satisfactory recovery (92.7 - 97.5% for aristolochic acid and 92.6 - 99.4% for aristolochic acid ) and an acceptable relative standard deviation ( © 2020
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Journal of Chromatography A
ISSN: 0021-9673
Year: 2020
Volume: 1627
4 . 7 5 9
JCR@2020
4 . 7 5 9
JCR@2020
ESI Discipline: CHEMISTRY;
ESI HC Threshold:70
CAS Journal Grade:2
Cited Count:
WoS CC Cited Count: 9
SCOPUS Cited Count: 16
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 14