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Author:

Zhang, W (Zhang, W.) | Wang, HJ (Wang, HJ.) | Jin, ZH (Jin, ZH.)

Indexed by:

SCIE Scopus EI

Abstract:

Macroporous silicon nitride (Si3N4) ceramics with high strength, uniform structure and relatively high porosity were obtained by gelcasting and carbonthermal reaction in a two-step sintering technique. Microstructure and composition were investigated by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD). Open porosity, pore size distribution and basic mechanical performance were measured by Archimedes method, mercury intrusion porosimetry and three-point bending methods, respectively. SEM and TEM results revealed that pores were formed by elongated beta-Si3N4. SADP measurement proved the formation of SiC particles. The SiC granules were beneficial for the formation of high ratio elongated beta-Si3N4, and at proper amount, they also acted as reinforcement phase. Thermodynamic analysis indicated that the mechanisms of the reactions were mainly associated with liquid-solid reaction and gas-liquid reaction.

Keyword:

ceramics silicon carbide silicon nitride X-ray diffraction

Author Community:

  • [ 1 ] Xian Jiaotong Univ, Sch Mat Sci & Engn, State Key Lab Mech Behav Mat, Xian 710049, Peoples R China

Reprint Author's Address:

  • Xian Jiaotong Univ, Sch Mat Sci & Engn, State Key Lab Mech Behav Mat, Xian 710049, Peoples R China.

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Source :

JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY

ISSN: 1005-0302

Year: 2005

Issue: 6

Volume: 21

Page: 894-898

0 . 1 7 5

JCR@2005

8 . 0 6 7

JCR@2020

ESI Discipline: MATERIALS SCIENCE;

JCR Journal Grade:2

CAS Journal Grade:2

Cited Count:

WoS CC Cited Count: 11

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count: -1

Chinese Cited Count: -1

30 Days PV: 5

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